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MassMS-NW-3426 cis-2,trans-4-hexadiene C6H10 (Mass of molecular ion: 82)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.2 26.0 2.2 27.0 13.5 28.0 1.2 29.0 3.4 37.0 1.6 38.0 3.3 39.0 29.1 40.0 5.6 41.0 35.2 42.0 5.9 50.0 4.9 51.0 7.2 52.0 3.8 53.0 17.7 54.0 17.0 55.0 6.7 56.0 1.2 63.0 2.1 65.0 9.5 66.0 4.3 67.0 100.0 68.0 5.7 77.0 4.1 78.0 1.0 79.0 10.4 80.0 1.5 81.0 12.8 82.0 51.7 83.0 3.2
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C6 H10 0.05 ml : 0.5 ml CDCl3 cis-2,trans-4-hexadiene 
Assign. Shift(ppm)
A 6.340 B 5.957 C 5.651 D 5.342 E 1.769 F 1.719 90MHZ : HSP-03-318 ASSIGNED BY C-H AND H-H COSY.
Hz ppm Int.2551.27 6.384 41 2549.68 6.380 120 2548.10 6.376 156 2546.88 6.373 127 2545.29 6.369 54 2540.28 6.357 49 2538.70 6.353 141 2537.11 6.349 186 2535.89 6.346 181 2534.55 6.342 184 2533.08 6.339 190 2531.86 6.336 151 2530.27 6.332 67 2525.27 6.319 54 2523.68 6.315 153 2522.09 6.311 200 2520.87 6.308 166 2519.29 6.304 75 2392.58 5.987 148 2392.09 5.986 150 2391.60 5.985 151 2391.11 5.984 154 2381.71 5.960 270 2381.23 5.959 272 2380.74 5.958 272 2380.00 5.956 280 2370.85 5.933 140 2370.36 5.932 144 2369.87 5.930 144 2369.38 5.929 146 2369.02 5.928 146 2276.86 5.698 79 2270.14 5.681 230 2263.43 5.664 245 2255.62 5.644 218 2255.13 5.643 226 2248.41 5.626 211 2241.70 5.610 77 2150.88 5.382 64 2144.53 5.367 170 2143.80 5.365 187 2141.11 5.358 71 2140.01 5.355 77 2139.28 5.353 80 2138.55 5.352 119 2137.82 5.350 176 2137.45 5.349 182 2136.72 5.347 197 2134.89 5.342 121 2133.06 5.338 183 2130.74 5.332 89 2130.37 5.331 86 2129.64 5.329 86 2128.91 5.327 70 2125.98 5.320 181 2118.90 5.302 66 710.94 1.779 962 710.45 1.778 969 709.84 1.777 961 709.35 1.775 902 704.22 1.763 923 703.61 1.761 954 703.13 1.760 959 702.51 1.758 919 696.17 1.742 70 692.38 1.733 908 691.77 1.731 925 691.16 1.730 936 690.55 1.728 972 685.30 1.715 896 684.69 1.714 929 684.08 1.712 946 683.47 1.711 1000
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1H NMR 89.56 MHz C6 H10 0.04 ml : 0.5 ml CDCl3 cis-2,trans-4-hexadiene Assign. Shift(ppm)
A 6.36 B 6.01 C 5.60 D 5.34 E 1.77 F 1.73 ASSIGNED BY C-H COSY.
Hz ppm Int.583.56 6.516 53 582.81 6.508 55 582.06 6.500 55 581.25 6.491 46 572.94 6.398 84 572.13 6.389 89 571.44 6.381 95 570.69 6.373 92 569.50 6.359 70 568.69 6.350 92 568.13 6.344 81 567.13 6.333 93 565.69 6.317 37 559.50 6.248 51 558.06 6.232 161 557.56 6.226 161 556.56 6.215 180 555.25 6.200 79 544.44 6.080 121 543.00 6.063 125 541.50 6.047 46 534.06 5.964 175 532.44 5.946 175 522.94 5.839 124 516.38 5.766 166 509.81 5.693 170 502.88 5.616 85 502.31 5.609 90 501.56 5.601 98 494.94 5.527 126 488.00 5.449 126 487.31 5.442 132 486.56 5.433 103 484.25 5.407 33 483.69 5.401 35 482.88 5.392 34 481.00 5.371 96 480.25 5.363 116 479.63 5.356 103 477.38 5.331 74 476.69 5.323 92 476.00 5.315 77 473.31 5.285 53 472.69 5.278 44 472.13 5.272 37 470.44 5.253 75 469.75 5.246 98 469.06 5.238 77 463.50 5.176 30 462.88 5.169 37 162.25 1.812 650 161.63 1.805 631 158.50 1.770 692 156.94 1.753 1000 156.38 1.747 973 155.13 1.733 657 151.56 1.693 599 151.00 1.687 625 150.50 1.681 620
in CDCl3
liquid film
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