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3,5-Dihydroxyacetophenone

Product Name 3,5-Dihydroxyacetophenone

CAS51863-60-6

MFC8H8O3

MW152.15

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  • Mass 

    MS-IW-0737          
3',5'-dihydroxyacetophenone
C8H8O3              (Mass of molecular ion:    152)


       Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV


          27.0       1.3
      28.0       1.1
      39.0       1.5
      43.0      11.4
      51.0       1.6
      53.0       2.8
      55.0       1.1
      63.0       1.1
      68.5       2.0
      69.0       9.2
      81.0       6.8
     109.0      46.9
     110.0       4.1
     137.0     100.0
     138.0       8.0
     152.0      99.8
     153.0       9.2
     154.0       1.1

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C8 H8 O3 0.039 g : 0.5 ml DMSO-d6
    3',5'-dihydroxyacetophenone
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             9.62
      B             6.813
      C             6.486
      D             2.481
  

         Hz     ppm     Int.


       3845.37   9.622    655
   2724.00   6.816    458
   2721.71   6.811    470
   2594.45   6.492    126
   2592.16   6.487    228
   2590.03   6.481    120
    991.52   2.481   1000

in DMSO-d6



KBr disc



nujol mull



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