400 MHz in DMSO-d6
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1H NMR 399.65 MHz C17 H19 N5 O6 S 0.041 g : 0.5 ml DMSO-d6 5'-o-tosyladenosine Assign. Shift(ppm)
A 8.248 B 8.110 C 7.730 D 7.36 E 7.35 F 5.896 G 5.62 J 5.46 K 4.650 L *1 4.345 M *1 4.301 N 4.241 P 4.088 Q 2.374 ASSIGNED BY H-H COSY.
Hz ppm Int.
3296.26 8.248 542 3241.33 8.111 558 3093.51 7.741 349 3086.91 7.725 132 3085.21 7.720 406 2945.92 7.372 329 2937.99 7.352 527 2359.13 5.903 221 2354.00 5.891 228 2249.15 5.628 252 2243.29 5.614 259 2183.59 5.464 249 2178.22 5.451 252 1866.58 4.671 59 1861.21 4.658 130 1855.83 4.644 132 1850.46 4.631 61 1746.34 4.370 50 1742.68 4.361 64 1735.47 4.343 139 1731.81 4.334 134 1725.95 4.319 119 1719.60 4.303 137 1714.97 4.292 56 1708.74 4.276 66 1702.64 4.261 57 1697.63 4.248 124 1692.75 4.236 128 1687.74 4.224 59 1641.36 4.107 58 1637.33 4.097 90 1635.25 4.092 87 1633.42 4.088 72 1630.98 4.082 85 1627.08 4.072 41 948.73 2.374 1000
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