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MS-NW-4318 1-chloro-2-methylpropene C4H7Cl (Mass of molecular ion: 90)
Source Temperature: 230 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.7 26.0 3.6 27.0 23.3 28.0 4.4 29.0 19.9 37.0 3.6 38.0 5.6 39.0 48.7 40.0 3.4 41.0 16.7 42.0 1.3 47.0 1.0 49.0 4.9 50.0 5.4 51.0 6.2 52.0 2.3 53.0 28.7 54.0 20.9 55.0 100.0 56.0 4.5 61.0 1.5 62.0 7.2 63.0 1.8 64.0 2.2 73.0 1.8 75.0 15.9 77.0 6.5 89.0 2.0 90.0 41.3 91.0 2.6 92.0 13.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H7 Cl 0.05 ml : 0.5 ml CDCl3 1-chloro-2-methylpropene Assign. Shift(ppm)
A 5.756 B *1 1.78 C *1 1.75
Hz ppm Int.
2305.18 5.768 33 2303.71 5.765 110 2302.12 5.761 231 2300.66 5.757 307 2299.19 5.754 255 2297.73 5.750 122 2296.26 5.746 32 710.08 1.777 706 708.62 1.774 915 699.83 1.752 659 699.34 1.750 737 698.85 1.749 611 697.75 1.746 1000
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