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MS-NW-7515 tripropyl phosphate C9H21O4P (Mass of molecular ion: 224)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
27.0 10.3 28.0 1.9 29.0 2.6 31.0 3.4 39.0 4.4 40.0 1.1 41.0 17.3 42.0 5.5 43.0 42.3 44.0 1.6 57.0 1.1 59.0 1.9 65.0 1.4 81.0 2.4 82.0 3.4 83.0 1.9 99.0 100.0 111.0 8.0 112.0 2.2 113.0 2.8 123.0 16.2 125.0 8.1 139.0 3.6 140.0 4.5 141.0 24.4 142.0 1.1 153.0 6.1 183.0 9.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H21 O4 P 0.05 ml : 0.5 ml CDCl3 tripropyl phosphate Assign. Shift(ppm)
A 4.003 B 1.717 C 0.974 J(P-31,A)=6.8HZ
Hz ppm Int.
1616.33 4.045 30 1611.08 4.032 256 1604.37 4.015 568 1597.17 3.997 559 1590.58 3.980 273 703.86 1.762 52 703.25 1.760 51 701.05 1.755 30 696.53 1.743 200 689.82 1.727 325 689.09 1.725 346 682.37 1.708 362 675.05 1.690 214 668.46 1.673 57 667.85 1.672 54 408.81 1.023 32 401.49 1.005 71 396.85 0.993 623 389.40 0.975 1000 384.77 0.963 66 381.96 0.956 611 377.56 0.945 51
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