4-ETHYL-1-HEXYN-3-OL

Mass

MS-NW-3531          
4-ethyl-1-hexyn-3-ol
C8H14O              (Mass of molecular ion:    126)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       1.0
      18.0       1.3
      26.0       2.2
      27.0      17.0
      28.0       1.4
      29.0      21.9
      38.0       1.0
      39.0       9.5
      40.0       1.3
      41.0      25.4
      42.0       7.3
      43.0     100.0
      44.0       3.2
      50.0       1.0
      51.0       2.3
      53.0       3.5
      54.0       1.0
      55.0      26.0
      56.0      19.1
      57.0       7.0
      65.0       1.2
      66.0       1.3
      67.0       2.9
      69.0       7.5
      70.0      17.9
      71.0      26.7
      72.0       2.3
      77.0       3.6
      79.0       3.6
      80.0       1.0
      81.0       1.2
      83.0       7.3
      84.0      13.5
      85.0       1.1
      91.0       1.0
      93.0       3.5
      95.0       1.4
      97.0       8.8
      98.0       4.4
     111.0       3.1

Assign. Shift(ppm) A 4.411 B 2.442 C 2.07 D 1.97 to 1.12 E 0.933 J(A,B)=2.2HZ.

     Hz     ppm     Int.

    398.50   4.450     91
    396.31   4.426    138
    394.25   4.403    140
    392.06   4.378    100
    219.88   2.456    763
    217.69   2.431    777
    185.31   2.070    563
    147.06   1.643     53
    145.56   1.626     40
    143.94   1.608     53
    142.75   1.594     53
    141.38   1.579     82
    138.88   1.551    120
    138.06   1.542    123
    137.13   1.532    142
    136.75   1.527    140
    135.56   1.514    189
    134.44   1.502    207
    131.19   1.465    304
    130.38   1.456    287
    129.94   1.451    283
    128.56   1.436    290
    126.06   1.408    131
    124.06   1.386    169
    122.25   1.366    113
    118.94   1.329     44
    117.63   1.314     37
    115.13   1.286     41
     94.94   1.061     32
     90.19   1.008    411
     89.44   0.999    381
     84.19   0.941    507
     83.44   0.932   1000
     81.00   0.905    213
     77.69   0.868    217
     76.81   0.858    289
     75.88   0.848    225
     74.25   0.830    105