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5111-65-9

2-Bromo-6-methoxynaphthalene

Product Name 2-Bromo-6-methoxynaphthalene

CAS5111-65-9

MFC11H9BrO

MW237.09

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  • 5111-65-9_ms
    Mass 

    MS-IW-4873          
2-bromo-6-methoxynaphthalene
C11H9BrO            (Mass of molecular ion:    236)


       Source Temperature: 130 °C
   Sample Temperature:  90 °C
   Direct, 75 eV


          39.0       1.0
      50.0       2.3
      51.0       1.6
      61.0       1.1
      62.0       4.0
      63.0       7.9
      64.0       1.6
      74.0       3.8
      75.0       3.1
      76.0       1.7
      86.0       2.6
      87.0       3.6
      88.0       5.0
      98.0       1.3
      99.0       1.4
     113.0       9.4
     114.0      26.2
     115.0       2.7
     118.0       3.3
     119.0       3.3
     126.0       9.1
     127.0       4.6
     128.0       2.9
     142.0       2.5
     156.0       1.1
     157.0       1.9
     193.0      41.1
     194.0       4.6
     195.0      40.1
     196.0       3.9
     206.0       2.0
     207.0       1.2
     208.0       1.9
     221.0      15.3
     222.0       2.0
     223.0      15.1
     224.0       1.7
     236.0     100.0
     237.0      12.4
     238.0      98.3
     239.0      11.9

400 MHz in CDCl3

  • 5111-65-9_1hnmr

    1H NMR 399.65 MHz
    C11 H9 Br O 0.039 g : 0.5 ml CDCl3
    2-bromo-6-methoxynaphthalene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.891
      B             7.612
      C             7.571
      D             7.482
      E             7.144
      F             7.066
      G             3.886
  

         Hz     ppm     Int.


       3154.79   7.894    126
   3153.08   7.890    125
   3047.00   7.625    111
   3037.84   7.602    123
   3031.25   7.585     93
   3022.46   7.563    143
   2994.51   7.493    126
   2992.55   7.488    119
   2985.84   7.472     80
   2983.76   7.466     78
   2860.84   7.159     95
   2858.28   7.152    107
   2851.81   7.136     86
   2849.24   7.130     99
   2825.07   7.069    126
   2822.63   7.063    108
   1553.34   3.887   1000

in CDCl3

  • 5111-65-9_13cnmr

KBr disc

  • 5111-65-9_ir1_2

nujol mull

  • 5111-65-9_ir2

  • 5111-65-9_raman

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