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51016-92-3More Spectrum > TRIMETHYLAMMONIUM TETRAPHENYLBORATE)(51016-92-3)13CNMR
TRIMETHYLAMMONIUM TETRAPHENYLBORATE)
Product Name TRIMETHYLAMMONIUM TETRAPHENYLBORATE)
CAS51016-92-3
MFC27H30BN
MW379.3448
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MS-NW-9773 trimethylamine tetraphenylborate C24H21B C3H9N (Mass of molecular ion: 379)
Source Temperature: 180 °C Sample Temperature: 140 °C Direct, 75 eV
15.0 1.1 17.0 3.3 18.0 16.5 27.0 1.0 28.0 5.3 29.0 1.1 30.0 7.0 32.0 1.1 37.0 1.6 38.0 1.4 39.0 5.1 41.0 1.0 42.0 5.9 43.0 2.2 50.0 6.1 51.0 8.2 52.0 9.4 56.0 1.1 57.0 2.2 58.0 30.0 59.0 15.6 60.0 1.3 61.0 4.4 63.0 2.6 74.0 3.0 75.0 1.4 76.0 3.2 77.0 14.0 78.0 65.2 79.0 4.4 85.0 1.5 86.0 1.3 87.0 4.8 93.5 1.2 105.5 1.2 106.0 1.1 106.5 1.3 107.0 1.3 111.0 1.6 112.0 2.9 113.0 9.4 118.0 1.0 118.5 3.0 119.0 2.7 119.5 1.1 120.0 1.1 120.5 1.4 121.0 2.9 136.0 3.6 137.0 14.8 138.0 2.9 139.0 5.1 161.0 2.8 162.0 9.4 163.0 57.4 164.0 100.0 165.0 52.1 166.0 5.9 213.0 1.5 237.0 2.1 238.0 2.1 239.0 2.9 240.0 9.1 241.0 15.4 242.0 46.8 243.0 9.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C24 H21 B 0.033 g : 0.5 ml DMSO-d6 trimethylamine tetraphenylborate Assign. Shift(ppm)
A 9.3 B 7.196 C 6.934 D 6.801 E 2.701
Hz ppm Int.
2884.83 7.219 38 2883.30 7.215 55 2882.23 7.212 60 2880.71 7.209 67 2879.64 7.206 69 2878.11 7.202 82 2876.89 7.199 103 2875.52 7.196 105 2874.15 7.192 85 2872.77 7.189 78 2871.55 7.186 76 2870.18 7.182 69 2868.96 7.179 61 2867.58 7.176 40 2779.08 6.954 102 2771.61 6.936 198 2764.13 6.917 117 2724.30 6.817 59 2717.13 6.799 90 2709.96 6.781 37 1079.71 2.702 1000
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