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MS-NW-3226 2-bromo-2-methylbutane C5H11Br (Mass of molecular ion: 150)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.9 26.0 2.3 27.0 21.1 28.0 1.9 29.0 28.1 36.0 1.0 37.0 1.2 38.0 2.8 39.0 24.8 40.0 3.8 41.0 41.6 42.0 15.8 43.0 95.6 44.0 3.4 50.0 2.3 51.0 2.9 52.0 1.2 53.0 7.5 54.0 2.0 55.0 59.2 56.0 3.6 67.0 1.6 69.0 3.7 70.0 17.6 71.0 100.0 72.0 5.8 80.0 1.8 81.0 1.0 82.0 1.9 121.0 2.8 123.0 2.8 149.0 1.1 151.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H11 Br 0.04 ml : 0.5 ml CDCl3 2-bromo-2-methylbutane Assign. Shift(ppm)
A 1.80 B 1.743 C 1.063
Hz ppm Int.
168.69 1.884 21 167.38 1.869 57 161.13 1.800 38 159.94 1.786 82 158.13 1.766 35 156.19 1.744 1000 154.13 1.721 49 153.63 1.716 49 152.56 1.704 41 102.44 1.144 48 101.75 1.137 86 101.19 1.130 54 94.94 1.061 202 94.25 1.053 100 88.06 0.984 35 87.31 0.975 59 86.44 0.966 31
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