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TETRAPHENYLARSONIUM CHLORIDE

Product Name TETRAPHENYLARSONIUM CHLORIDE

CAS507-28-8

MFC24H20As.Cl

MW418.79

Mass

MS-NW-7345          
tetraphenylarsonium chloride
C24H20AsCl H2O      (Mass of molecular ion:    418)

   Source Temperature: 200 °C
   Sample Temperature: 230 °C
   Direct, 75 eV

      18.0       1.4
      36.0       3.3
      38.0       1.1
      39.0       1.7
      50.0       2.6
      51.0       6.8
      52.0       1.4
      63.0       1.0
      74.0       1.1
      75.0       1.1
      76.0       1.2
      77.0       7.2
      78.0       7.7
     100.0       1.0
     101.0       1.5
     102.0       1.0
     112.0       3.3
     114.0       1.1
     115.0       1.9
     125.0       1.4
     126.0       1.1
     128.0       1.9
     151.0      12.5
     152.0     100.0
     153.0       9.5
     154.0      14.3
     155.0       1.9
     214.0       1.0
     227.0      30.4
     228.0       6.4
     229.0       8.2
     230.0       2.9
     306.0      37.8
     307.0       7.8
     382.0       1.9
     383.0       4.2
     384.0       1.1

400 MHz in D2O

¹H NMR	399.65 MHz
C₂₄ H₂₀ As Cl	0.042 g : 0.5 ml D₂O
tetraphenylarsonium chloride

    Assign.     Shift(ppm)

      A             7.944
      B             7.784
      C             7.729

     Hz     ppm     Int.

   3184.20   7.968    127
   3182.83   7.965    236
   3181.61   7.961    151
   3179.17   7.955     48
   3177.19   7.950    171
   3175.35   7.946    504
   3173.68   7.942    224
   3169.40   7.931    205
   3168.03   7.928    372
   3166.66   7.924    220
   3125.46   7.821     32
   3123.63   7.816     43
   3119.51   7.806    476
   3117.83   7.802    262
   3111.42   7.786   1000
   3105.77   7.772    232
   3103.64   7.766    788
   3099.37   7.756     61
   3098.91   7.755     59
   3092.04   7.737    850
   3091.13   7.735    982
   3085.78   7.722    197
   3083.95   7.717    544
   3082.58   7.714    429

KBr disc

nujol mull

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