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1,8-Bis(chloromethyl)naphthalene

Product Name 1,8-Bis(chloromethyl)naphthalene

CAS50585-29-0

MFC12H10Cl2

MW225.11

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¹HNMR

¹³CNMR

Mass

MS-IW-0633          
1,8-bis(chloromethyl)naphthalene
C12H10Cl2           (Mass of molecular ion:    224)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      36.0       2.1
      50.0       1.2
      51.0       2.3
      62.0       1.2
      63.0       7.1
      64.0       2.7
      74.0       1.3
      75.0       4.2
      75.5       5.1
      76.0      26.8
      76.5       9.9
      77.0       4.6
      94.0       1.5
     115.0       1.3
     126.0       1.7
     127.0       1.7
     139.0       1.8
     141.0       3.1
     142.0       1.6
     150.0       3.3
     151.0       8.1
     152.0      27.0
     153.0      36.4
     154.0      15.3
     155.0       3.2
     169.0       1.4
     170.0       3.5
     187.0       8.4
     188.0       1.7
     189.0     100.0
     190.0      13.9
     191.0      32.3
     192.0       4.5
     224.0      31.9
     225.0       4.5
     226.0      21.0
     227.0       2.8
     228.0       3.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₀ Cl₂	0.022 g : 0.5 ml CDCl₃
1,8-bis(chloromethyl)naphthalene

    Assign.     Shift(ppm)

      A             7.897
      B             7.602
      C             7.464
      D             5.324

     Hz     ppm     Int.

   3161.13   7.910    129
   3159.79   7.907    141
   3152.83   7.889    144
   3151.49   7.886    156
   3042.97   7.615    123
   3041.50   7.611    126
   3035.89   7.597    155
   3034.42   7.593    165
   2990.23   7.483    154
   2983.15   7.465    142
   2982.06   7.462    174
   2974.98   7.444    113
   2128.05   5.325   1000

in CDCl3

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