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MS-IW-9210 azetidine C3H7N (Mass of molecular ion: 57)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.6 18.0 1.8 26.0 8.1 26.5 2.0 27.0 16.3 28.0 100.0 29.0 78.9 30.0 52.9 31.0 2.4 38.0 1.0 39.0 1.8 40.0 1.7 41.0 3.2 42.0 7.4 44.0 1.0 51.0 1.5 52.0 2.4 54.0 3.6 55.0 1.5 56.0 35.0 57.0 80.2 58.0 3.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C3 H7 N 0.05 ml : 0.5 ml CDCl3 azetidine Assign. Shift(ppm)
A 3.628 B 2.327 C 2.08
Hz ppm Int.
1457.52 3.647 797 1450.20 3.629 1000 1445.56 3.618 89 1442.75 3.611 781 945.07 2.365 159 941.89 2.357 28 940.92 2.355 36 937.62 2.347 421 935.18 2.340 48 933.72 2.337 50 930.30 2.328 526 926.76 2.319 46 925.66 2.317 44 922.85 2.310 360 919.68 2.302 30 918.58 2.299 23 915.53 2.291 146 829.35 2.076 238
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