-
MassMS-NW-7174 1-chloroanthracene C14H9Cl (Mass of molecular ion: 212)
Source Temperature: 210 °C Sample Temperature: 180 °C Reservoir, 75 eV
50.0 1.2 51.0 1.3 62.0 1.8 63.0 1.6 74.0 2.6 75.0 6.6 75.5 1.8 76.0 1.7 86.0 1.1 87.0 4.6 87.5 2.7 88.0 16.8 88.5 4.0 93.0 4.4 94.0 1.5 98.0 1.4 99.0 1.4 106.0 14.7 106.5 2.6 107.0 4.7 126.0 1.3 149.0 1.4 150.0 5.2 151.0 6.8 152.0 1.2 174.0 3.6 175.0 5.0 176.0 24.3 177.0 11.3 178.0 2.4 212.0 100.0 213.0 15.7 214.0 33.8 215.0 5.4
400 MHz in CDCl3
-
1H NMR 399.65 MHz C14 H9 Cl 0.038 g : 0.5 ml CDCl3 1-chloroanthracene 
Assign. Shift(ppm)
A 8.785 B 8.367 C *1 8.033 D *1 7.953 E 7.864 F 7.529 G *2 7.49 J *2 7.47 K 7.306 ASSIGNED BY H-H AND C-H COSY.
Hz ppm Int.3510.99 8.786 950 3503.78 8.768 31 3502.69 8.765 30 3502.08 8.763 32 3344.12 8.368 1000 3215.09 8.045 313 3211.79 8.037 305 3209.96 8.032 261 3205.44 8.021 342 3184.20 7.968 329 3179.08 7.955 276 3177.73 7.952 321 3174.56 7.944 332 3147.46 7.876 514 3138.92 7.855 552 3023.56 7.566 30 3022.71 7.564 30 3013.43 7.541 576 3006.35 7.523 687 2997.44 7.501 213 2993.53 7.491 911 2990.97 7.484 587 2989.62 7.481 591 2987.55 7.476 600 2986.21 7.473 538 2983.76 7.466 829 2981.08 7.460 164 2979.74 7.456 150 2975.34 7.445 46 2974.00 7.442 38 2972.29 7.438 32 2927.73 7.326 473 2920.41 7.308 656 2918.70 7.304 836 2912.11 7.287 379
in CDCl3
KBr disc
More Suppliers
