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4975-73-9More Spectrum > N,N'-Dicyclohexyl-4-morpholinecarboxamidine (4975-73-9)IR2
N,N'-Dicyclohexyl-4-morpholinecarboxamidine
Product Name N,N'-Dicyclohexyl-4-morpholinecarboxamidine
CAS4975-73-9
MFC17H31N3O
MW293.45
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MS2014-05050CW N,N'-dicyclohexyl-4-morpholinecarboxamidine C17H31N3O (Mass of molecular ion: 293)
Source Temperature: 240 °C Sample Temperature: 20 °C Direct, 70 eV
17.0 2.3 18.0 10.7 27.0 5.5 28.0 8.5 29.0 10.5 30.0 7.4 39.0 7.5 40.0 1.3 41.0 49.6 42.0 15.9 43.0 44.4 44.0 7.7 45.0 11.6 53.0 7.0 54.0 9.5 55.0 75.0 56.0 28.4 57.0 16.2 58.0 5.5 59.0 1.1 60.0 1.7 65.0 1.3 66.0 1.0 67.0 9.9 68.0 6.3 69.0 43.6 70.0 6.5 71.0 2.8 72.0 9.3 73.0 4.0 74.0 1.0 77.0 1.6 79.0 5.3 80.0 2.9 81.0 20.6 82.0 9.8 83.0 36.6 84.0 12.8 85.0 5.5 86.0 42.5 87.0 17.5 88.0 7.9 94.0 1.6 95.0 4.5 96.0 5.0 97.0 6.1 98.0 90.9 99.0 47.5 100.0 4.3 101.0 10.5 102.0 1.4 107.0 1.0 108.0 1.7 109.0 3.0 110.0 100.0 111.0 10.3 112.0 4.4 113.0 59.2 114.0 9.5 115.0 4.5 121.0 1.1 122.0 1.3 123.0 5.9 124.0 6.2 125.0 32.7 126.0 9.3 127.0 10.1 128.0 3.2 129.0 19.1 130.0 14.3 131.0 1.0 136.0 1.6 137.0 1.7 138.0 5.3 139.0 6.4 140.0 6.7 141.0 3.7 142.0 1.6 150.0 1.0 151.0 3.4 152.0 4.1 153.0 37.3 154.0 25.1 155.0 4.1 156.0 1.4 163.0 3.2 164.0 2.1 165.0 5.3 166.0 10.3 167.0 6.1 168.0 13.0 169.0 3.0 177.0 1.3 178.0 1.8 179.0 1.5 180.0 6.5 181.0 15.8 182.0 5.9 183.0 3.6 192.0 1.9 193.0 3.2 194.0 5.0 195.0 8.1 196.0 14.4 197.0 2.8 206.0 2.2 207.0 7.9 208.0 17.3 209.0 3.8 210.0 4.3 211.0 27.8 212.0 10.1 213.0 1.2 220.0 4.8 221.0 2.0 222.0 29.4 223.0 9.1 224.0 1.6 234.0 2.1 236.0 16.1 237.0 4.6 238.0 2.6 248.0 7.7 249.0 1.9 250.0 85.7 251.0 14.7 252.0 2.3 262.0 2.1 263.0 4.7 264.0 7.6 265.0 1.9 278.0 2.1 290.0 2.1 292.0 6.0 293.0 33.8 294.0 7.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C17 H31 N3 O 0.040 g : 0.5 ml CDCl3 N,N'-dicyclohexyl-4-morpholinecarboxamidine Assign. Shift(ppm)
A 3.675 B 3.079 C *1 3.00 D *1 2.90 E *2 1.91 F 1.75 G *2 1.65 to 1.55 J *3 1.33 K 1.29 L 1.19 M *3 1.062 ASSIGNED BY H-H AND C-H COSY.
Hz ppm Int.
1473.88 3.688 805 1469.24 3.677 1000 1464.48 3.665 909 1235.47 3.092 778 1230.59 3.080 929 1225.95 3.068 772 1217.29 3.046 33 1211.67 3.032 50 1207.89 3.023 81 1203.86 3.013 62 1201.05 3.006 90 1197.27 2.996 150 1193.48 2.987 96 1190.55 2.979 66 1186.52 2.969 86 1183.11 2.961 52 1182.74 2.960 52 1172.73 2.935 30 1169.19 2.926 68 1168.82 2.925 68 1165.04 2.916 86 1163.57 2.912 87 1161.87 2.908 81 1159.30 2.901 129 1155.40 2.892 112 1150.88 2.880 57 1149.29 2.876 66 1145.51 2.867 44 769.29 1.925 172 766.72 1.919 187 762.57 1.909 128 762.08 1.907 129 761.72 1.906 128 757.08 1.895 198 756.10 1.892 194 754.15 1.888 200 704.71 1.764 413 701.66 1.756 307 700.68 1.754 306 700.20 1.753 305 694.95 1.739 355 691.77 1.731 356 655.52 1.641 114 650.88 1.629 161 647.71 1.621 187 638.67 1.599 284 636.60 1.593 295 636.11 1.592 294 630.49 1.578 203 629.76 1.576 201 625.37 1.565 286 617.19 1.545 32 612.06 1.532 30 611.69 1.531 30 550.90 1.379 59 539.18 1.350 202 536.38 1.343 198 527.95 1.322 460 524.17 1.312 358 520.14 1.302 459 510.74 1.278 346 508.18 1.272 347 506.84 1.269 419 501.95 1.256 119 498.54 1.248 192 495.73 1.241 182 489.14 1.224 76 487.30 1.220 70 481.69 1.206 159 478.64 1.198 126 472.41 1.183 131 469.36 1.175 196 460.82 1.154 84 460.57 1.153 84 457.28 1.145 123 454.22 1.137 71 448.49 1.123 33 442.50 1.108 102 439.33 1.100 96 436.28 1.092 38 430.05 1.077 200 427.73 1.071 195 419.31 1.050 180 416.63 1.043 183 410.77 1.028 36 407.71 1.021 69 404.42 1.012 66 404.17 1.012 66
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