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MassMS-NW-8769 endo-norborneol C7H12O (Mass of molecular ion: 112)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.1 27.0 13.2 28.0 3.3 29.0 12.7 31.0 4.2 38.0 1.2 39.0 20.2 40.0 6.3 41.0 31.8 42.0 7.2 43.0 12.2 44.0 6.4 45.0 7.3 50.0 1.1 51.0 2.9 52.0 1.4 53.0 14.5 54.0 6.0 55.0 25.6 56.0 12.4 57.0 35.0 58.0 5.0 65.0 6.0 66.0 61.2 67.0 95.6 68.0 74.8 69.0 10.2 70.0 15.3 71.0 7.1 77.0 7.2 78.0 2.4 79.0 100.0 80.0 7.6 81.0 15.8 82.0 2.1 83.0 20.6 84.0 5.3 91.0 2.8 93.0 7.2 94.0 91.2 95.0 12.6 97.0 6.4 111.0 1.5 112.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H12 O 0.046 g : 0.5 ml CDCl3 endo-norborneol 
Assign. Shift(ppm)
A 4.216 B 2.24 C 2.16 D 2.07 E 1.94 F 1.88 G 1.56 J 1.37 K 1.34 L 1.30 M 1.29 N 0.843 ASSIGNED BY H-H AND C-H COSY.
Hz ppm Int.1694.21 4.240 162 1692.99 4.237 179 1689.82 4.229 286 1686.52 4.220 193 1684.69 4.216 230 1682.86 4.211 196 1679.69 4.203 285 1676.27 4.195 167 1674.93 4.191 155 900.02 2.253 302 895.75 2.242 529 891.60 2.231 288 868.41 2.173 269 864.26 2.163 493 859.62 2.151 295 852.54 2.134 46 852.17 2.133 44 850.34 2.128 37 826.54 2.069 702 789.31 1.976 205 786.25 1.968 235 784.42 1.963 206 781.37 1.956 215 779.05 1.950 219 776.12 1.942 383 774.17 1.938 250 773.32 1.935 297 771.36 1.931 356 768.55 1.924 239 765.99 1.917 328 763.06 1.910 392 761.23 1.905 280 759.89 1.902 142 758.30 1.898 240 756.71 1.894 198 754.27 1.888 227 753.30 1.885 230 751.46 1.881 259 749.88 1.877 249 749.51 1.876 249 746.83 1.869 165 744.26 1.863 197 742.07 1.857 193 738.04 1.847 111 735.84 1.842 155 642.70 1.609 58 639.40 1.600 71 638.79 1.599 76 636.60 1.593 101 635.74 1.591 87 633.54 1.586 111 632.32 1.583 108 629.52 1.576 226 625.24 1.565 322 622.07 1.557 298 617.19 1.545 174 613.53 1.536 223 610.35 1.528 155 609.25 1.525 210 606.08 1.517 116 564.58 1.413 40 561.28 1.405 50 558.72 1.399 155 557.25 1.395 167 554.44 1.388 275 552.98 1.384 284 549.68 1.376 233 547.97 1.372 334 546.02 1.367 500 544.56 1.363 389 542.24 1.357 482 540.65 1.353 465 537.72 1.346 736 536.01 1.342 1000 534.06 1.337 682 532.59 1.333 431 529.17 1.325 388 527.34 1.320 505 525.15 1.315 345 523.07 1.309 309 520.63 1.303 193 519.17 1.300 369 517.58 1.296 636 515.87 1.291 660 514.04 1.287 637 512.33 1.282 365 509.40 1.275 174 507.69 1.271 277 505.98 1.267 285 504.27 1.262 286 502.56 1.258 158 346.44 0.867 338 343.02 0.859 593 339.60 0.850 311 333.62 0.835 317 330.08 0.826 548 326.66 0.818 282
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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