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MassMS-NW-2851 trans-decalin C10H18 (Mass of molecular ion: 138)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 11.5 28.0 2.4 29.0 9.8 39.0 17.4 40.0 3.0 41.0 42.1 42.0 4.0 43.0 3.3 51.0 2.7 52.0 1.6 53.0 10.3 54.0 15.7 55.0 30.9 56.0 2.7 57.0 1.0 65.0 3.2 66.0 8.9 67.0 85.2 68.0 90.6 69.0 44.1 70.0 3.9 77.0 4.3 78.0 1.2 79.0 8.3 80.0 4.9 81.0 56.5 82.0 68.1 83.0 14.6 91.0 2.2 93.0 3.5 94.0 4.5 95.0 65.3 96.0 68.0 97.0 9.1 109.0 18.6 110.0 8.5 123.0 1.2 137.0 1.7 138.0 100.0 139.0 11.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H18 0.016 g : 0.5 ml CDCl3 trans-decalin 
Assign. Shift(ppm)
A 1.673 B 1.545 C 1.231 D 0.93 E 0.87 ASSIGNED BY H-H AND C-H COSY.
Hz ppm Int.688.96 1.724 55 688.11 1.722 68 687.62 1.721 69 687.13 1.720 70 684.94 1.714 99 684.45 1.713 94 683.84 1.712 103 683.47 1.711 104 682.74 1.709 111 681.15 1.705 124 680.79 1.704 123 675.17 1.690 810 672.85 1.684 912 670.41 1.678 673 665.89 1.667 930 664.18 1.662 909 663.82 1.662 910 661.38 1.655 504 658.81 1.649 165 656.98 1.644 135 654.05 1.637 122 652.22 1.632 89 651.12 1.630 129 646.36 1.618 45 632.32 1.583 44 624.27 1.563 787 623.41 1.560 780 613.28 1.535 874 611.69 1.531 994 602.42 1.508 50 601.81 1.506 48 601.07 1.504 45 600.59 1.503 45 599.98 1.502 49 599.24 1.500 49 598.63 1.498 47 597.66 1.496 47 516.36 1.293 87 515.26 1.290 75 514.65 1.288 70 514.16 1.287 67 512.82 1.284 93 511.72 1.281 81 509.64 1.276 46 509.16 1.275 45 508.54 1.273 55 507.20 1.270 80 501.34 1.255 581 499.27 1.250 308 498.29 1.247 338 495.24 1.240 487 492.31 1.232 1000 488.89 1.224 578 486.45 1.218 352 483.28 1.210 542 481.45 1.205 455 479.86 1.201 439 475.59 1.191 59 473.88 1.186 64 471.44 1.180 94 470.34 1.177 97 469.12 1.174 78 467.90 1.171 127 394.53 0.988 49 394.17 0.987 51 391.36 0.980 148 389.04 0.974 198 387.57 0.970 182 386.35 0.967 181 385.99 0.966 178 380.74 0.953 419 380.13 0.952 415 377.69 0.946 470 376.34 0.942 373 376.10 0.942 373 375.24 0.939 357 374.15 0.937 365 371.83 0.931 351 368.29 0.922 614 365.23 0.914 559 361.69 0.906 343 361.21 0.904 343 359.25 0.899 448 356.57 0.893 569 353.76 0.886 702 351.68 0.880 547 349.37 0.875 332 346.56 0.868 207 345.34 0.865 236 343.02 0.859 304 340.45 0.852 260 338.13 0.847 144 335.21 0.839 99 334.84 0.838 97 334.47 0.837 104 333.98 0.836 102 332.52 0.833 103 329.71 0.825 59
in CDCl3
liquid film
4880 A,200 M,liquid
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