cis-9-oxabicyclo[6.1.0]nonane
Product Name cis-9-oxabicyclo[6.1.0]nonane
CAS4925-71-7
MFC8H14O
MW126.2
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MassMS-NW-8689 cis-9-oxabicyclo(6.1.0)nonane C8H14O (Mass of molecular ion: 126)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.0 26.0 1.2 27.0 18.3 28.0 5.1 29.0 21.2 31.0 1.8 38.0 1.0 39.0 21.5 40.0 3.7 41.0 68.8 42.0 26.6 43.0 16.8 44.0 4.8 45.0 1.3 51.0 1.6 53.0 6.7 54.0 34.1 55.0 100.0 56.0 25.9 57.0 44.4 58.0 7.3 59.0 2.0 65.0 1.7 66.0 1.8 67.0 53.2 68.0 9.3 69.0 16.9 70.0 14.2 71.0 9.1 72.0 11.2 77.0 1.6 79.0 7.6 80.0 5.1 81.0 7.5 82.0 13.8 83.0 28.3 84.0 13.5 85.0 3.1 91.0 1.0 93.0 5.9 95.0 2.2 97.0 19.2 98.0 14.8 99.0 1.5 111.0 6.3 126.0 2.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H14 O 0.043 g : 0.5 ml CDCl3 cis-9-oxabicyclo[6.1.0]nonane 
Assign. Shift(ppm)
A 2.89 B *1 2.13 C *1 1.88 to 0.95
Hz ppm Int.268.63 3.000 71 266.25 2.973 131 264.50 2.954 218 256.88 2.869 267 254.06 2.837 214 197.50 2.206 182 187.00 2.088 165 157.38 1.758 58 136.56 1.525 862 134.06 1.497 1000 108.13 1.208 96 98.81 1.104 33 97.25 1.086 34
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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