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MassMS-IW-0564 2-methyl-3-nitroanisole C8H9NO3 (Mass of molecular ion: 167)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 1.0 27.0 2.2 28.0 2.6 30.0 1.1 38.0 1.5 39.0 11.4 40.0 1.2 41.0 2.9 43.0 2.0 50.0 5.9 51.0 19.3 52.0 15.3 53.0 5.3 55.0 1.6 59.0 1.4 62.0 2.3 63.0 9.6 64.0 3.9 65.0 29.9 66.0 5.0 67.0 2.0 74.0 1.4 75.0 1.9 76.0 3.5 77.0 31.0 78.0 30.2 79.0 8.6 80.0 1.5 89.0 7.1 90.0 14.8 91.0 56.6 92.0 100.0 93.0 9.7 94.0 4.6 95.0 7.2 105.0 17.4 106.0 16.0 107.0 7.7 108.0 2.1 120.0 1.9 121.0 1.6 122.0 5.8 135.0 7.9 150.0 77.6 151.0 7.7 167.0 52.0 168.0 5.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H9 N O3 0.038 g : 0.5 ml CDCl3 2-methyl-3-nitroanisole 
Assign. Shift(ppm)
A 7.383 B 7.259 C 7.042 D 3.885 E 2.349
Hz ppm Int.2955.32 7.395 81 2954.22 7.393 86 2947.14 7.375 114 2946.04 7.372 118 2909.55 7.281 65 2909.06 7.280 75 2901.37 7.260 117 2900.76 7.259 137 2893.07 7.240 57 2892.58 7.238 67 2818.12 7.052 104 2817.75 7.051 104 2810.30 7.032 84 2809.94 7.032 87 2809.57 7.031 86 1552.61 3.885 1000 938.72 2.349 763
in CDCl3
KBr disk
Nujol
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