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MassMS-IW-4188 p-(dichloromethyl)fluorobenzene C7H5Cl2F (Mass of molecular ion: 178)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
50.0 1.1 53.5 1.2 57.0 3.6 61.0 1.5 62.0 1.6 63.0 1.4 71.0 1.0 71.5 2.5 79.0 1.0 81.0 2.4 83.0 2.8 95.0 1.2 107.0 12.9 108.0 5.1 109.0 1.1 117.0 2.8 123.0 1.8 143.0 100.0 144.0 8.0 145.0 32.3 146.0 2.5 177.0 1.3 178.0 6.8 179.0 1.4 180.0 4.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H5 Cl2 F 0.05 ml : 0.5 ml CDCl3 p-(dichloromethyl)fluorobenzene 
Assign. Shift(ppm)
A 7.537 B 7.052 C 6.678
Hz ppm Int.3021.39 7.561 61 3018.34 7.553 473 3016.05 7.547 196 3013.31 7.540 470 3011.17 7.535 264 3009.34 7.530 532 3006.44 7.523 213 3004.30 7.518 505 3001.25 7.510 71 2829.90 7.081 73 2826.84 7.074 553 2824.55 7.068 173 2821.50 7.060 94 2820.13 7.057 219 2818.30 7.052 806 2816.31 7.047 211 2814.79 7.044 89 2811.74 7.036 180 2809.45 7.030 504 2806.40 7.023 70 2668.91 6.679 1000
in CDCl3
liquid film
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