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MS-IW-8154 4-fluoro-o-xylene C8H9F (Mass of molecular ion: 124)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.2 39.0 2.0 50.0 1.9 51.0 4.6 57.0 2.8 60.0 1.2 61.0 1.6 62.0 1.0 63.0 2.0 70.0 1.1 74.0 1.1 75.0 2.6 77.0 7.1 81.0 1.3 83.0 6.0 95.0 2.0 96.0 3.8 97.0 2.9 101.0 4.3 102.0 1.4 103.0 7.6 107.0 1.7 109.0 100.0 110.0 7.9 120.0 1.0 121.0 3.1 122.0 2.8 123.0 30.2 124.0 56.1 125.0 5.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H9 F 0.05 ml : 0.5 ml CDCl3 4-fluoro-o-xylene Assign. Shift(ppm)
A 7.002 B 6.794 C 6.740 D *1 2.188 E *1 2.163
Hz ppm Int.
2806.03 7.022 111 2799.93 7.006 127 2797.73 7.001 137 2791.75 6.986 126 2721.44 6.810 120 2718.75 6.803 140 2711.79 6.786 120 2709.11 6.779 141 2703.13 6.764 92 2700.32 6.757 73 2694.58 6.743 155 2691.89 6.736 123 2686.16 6.722 77 2683.47 6.715 62 874.39 2.188 1000 864.62 2.164 851
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