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449-55-8

6,11-DIHYDRO-5H-DIBENZO[B,E]AZEPINE

Product Name 6,11-DIHYDRO-5H-DIBENZO[B,E]AZEPINE

CAS449-55-8

MFC14H13N

MW195.26

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  • 449-55-8_ms_1
    Mass

    MS-NW-6329          
    6,11-dihydro-5H-dibenz(b,E)azepine
    C14H13N             (Mass of molecular ion:    195)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          17.0       2.4
          18.0      11.0
          27.0       1.5
          38.0       1.2
          39.0       5.5
          43.0       1.1
          50.0       3.1
          51.0       5.5
          52.0       1.5
          62.0       2.4
          63.0       6.0
          64.0       1.9
          65.0       3.5
          66.0       3.3
          69.0       1.2
          69.5       3.4
          70.0       1.3
          70.5       1.6
          74.0       1.9
          75.0       2.2
          76.0       2.4
          77.0       4.6
          78.0       1.4
          81.0       1.3
          81.5       2.9
          82.0       6.0
          82.5       7.9
          83.0       2.8
          83.5       8.6
          84.0       1.7
          86.0       1.0
          87.0       1.8
          88.0       1.3
          89.0       6.0
          90.0       5.8
          91.0       4.5
          95.5       6.6
          96.0       2.2
          96.5      13.3
          97.0       3.3
          97.5       3.7
          98.0       1.2
         101.0       1.0
         102.0       1.2
         113.0       1.4
         114.0       1.1
         115.0       4.2
         116.0       6.1
         117.0       4.7
         118.0      12.1
         119.0       1.3
         126.0       1.2
         127.0       1.4
         128.0       2.6
         139.0       5.3
         140.0       2.4
         141.0       1.0
         149.0       1.0
         150.0       1.4
         151.0       2.3
         152.0       5.4
         153.0       2.0
         154.0       1.1
         163.0       5.1
         164.0       6.1
         165.0      27.8
         166.0       9.0
         167.0       7.0
         168.0       1.9
         176.0       2.0
         177.0       5.2
         178.0      13.2
         179.0      10.4
         180.0       6.2
         190.0       6.6
         191.0       9.0
         192.0      31.2
         193.0      92.4
         194.0     100.0
         195.0      78.0
         196.0      11.5
    

400 MHz in DMSO-d6

  • 449-55-8_1hnmr_0

    1H NMR 399.65 MHz
    C14 H13 N 0.038 g : 0.5 ml DMSO-d6
    6,11-dihydro-5H-dibenz(b,e)azepine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.20 B 6.887 C 6.813 D 6.38 E 6.37 F 5.89 G 4.398 J 4.095

         Hz     ppm     Int.
    

       2891.60   7.236     30
       2889.40   7.230     57
       2888.18   7.227    103
       2886.35   7.223    123
       2885.01   7.219    213
       2882.20   7.212    174
       2879.15   7.205    513
       2877.20   7.200    680
       2875.98   7.197   1000
       2875.24   7.195    775
       2873.54   7.191    313
       2871.83   7.186    279
       2870.73   7.184    212
       2869.63   7.181    110
       2866.58   7.173    136
       2755.37   6.895    181
       2747.92   6.876    188
       2731.57   6.835    116
       2729.98   6.831    111
       2724.24   6.817    179
       2723.63   6.816    185
       2722.41   6.812    197
       2716.43   6.798    139
       2714.72   6.793    121
       2558.11   6.401    139
       2556.88   6.398    183
       2549.68   6.380    643
       2543.46   6.365    112
       2541.75   6.360    330
       2357.79   5.900     92
       2352.66   5.887    173
       2349.73   5.880     64
       2347.66   5.875     90
       1760.50   4.406    604
       1755.37   4.393    600
       1636.60   4.096    910
    

in DMSO-d6

  • 449-55-8_13cnmr_0

KBr disc

  • 449-55-8_ir1_2

nujol mull

  • 449-55-8_ir2_1