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WebSite > CAS DataBase List >  4441-17-2More Spectrum > 1,1',1''-phosphinoylidynetripiperidine(4441-17-2)1HNMR

1,1',1''-phosphinoylidynetripiperidine

Product Name 1,1',1''-phosphinoylidynetripiperidine

CAS4441-17-2

MFC15H30N3OP

MW299.39


  • Mass 

    MS-NW-7996          
tripiperidinophosphine oxide
C15H30N3OP          (Mass of molecular ion:    299)


       Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV


          18.0       1.6
      28.0       1.7
      29.0       1.5
      30.0       2.9
      41.0       2.6
      42.0       3.5
      44.0       1.2
      55.0       4.2
      56.0       4.0
      70.0       1.0
      76.0       1.8
      82.0       2.1
      83.0       8.7
      84.0     100.0
      85.0      20.9
      86.0       4.0
     115.0       1.1
     130.0       1.2
     131.0       2.8
     132.0       2.9
     214.0       4.5
     215.0      13.0
     216.0       2.8
     299.0       8.5
     300.0       3.1

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H30 N3 O P 0.048 g : 0.5 ml CDCl3
    tripiperidinophosphine oxide
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             3.039
      B             1.56
      C             1.50
  

         Hz     ppm     Int.


       1222.53   3.060    546
   1216.67   3.045   1000
   1211.91   3.033    883
   1206.18   3.019    461
    640.14   1.602     57
    637.70   1.596     78
    634.89   1.589    174
    627.20   1.570    370
    622.56   1.558    412
    618.90   1.549    303
    610.35   1.528    392
    604.61   1.513    697
    599.85   1.501    765
    595.95   1.492    461
    588.99   1.474    162

in CDCl3



liquid film



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