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MassMS-NW-8810 alpha,alpha,alpha-trifluoro-o-iodotoluene C7H4F3I (Mass of molecular ion: 272)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 1.2 50.0 7.5 51.0 2.3 57.0 1.8 69.0 3.9 74.0 4.7 75.0 12.3 76.0 3.7 94.0 1.8 95.0 17.0 96.0 1.1 99.0 2.4 119.0 1.7 125.0 9.9 126.0 4.6 127.0 2.9 136.0 2.8 143.0 1.6 144.0 2.5 145.0 87.4 146.0 6.7 253.0 4.9 272.0 100.0 273.0 7.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H4 F3 I 0.05 ml : 0.5 ml CDCl3 alpha,alpha,alpha-trifluoro-o-iodotoluene 
Assign. Shift(ppm)
A 7.990 B 7.614 C 7.410 D 7.165 CONFIRMED BY LAOCN PROGRAM
Hz ppm Int.720.50 8.045 674 720.00 8.040 731 719.31 8.032 678 716.19 7.997 142 712.38 7.955 876 712.06 7.951 870 704.44 7.866 53 704.00 7.861 52 692.25 7.730 51 688.31 7.686 445 686.44 7.665 489 680.50 7.599 993 680.06 7.594 865 678.56 7.577 1000 674.25 7.529 134 671.88 7.503 405 671.25 7.495 490 670.56 7.488 498 669.88 7.480 405 664.63 7.422 689 663.88 7.413 833 663.31 7.407 817 662.63 7.399 662 656.88 7.335 390 656.19 7.327 457 655.50 7.320 429 654.75 7.311 336 652.63 7.288 112 652.06 7.281 114 649.19 7.249 555 648.63 7.243 567 646.63 7.221 541 641.38 7.162 676 640.81 7.156 624 639.56 7.142 617 634.13 7.081 275 633.50 7.074 284 632.88 7.067 229 632.19 7.059 251 631.63 7.053 235 629.25 7.027 59
in CDCl3
liquid film
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