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MS-NW-3359 N-ethyl-tert-butylamine C6H15N (Mass of molecular ion: 101)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.4 18.0 2.4 27.0 4.5 28.0 3.3 29.0 7.8 30.0 16.9 39.0 3.9 41.0 10.7 42.0 9.1 43.0 1.4 44.0 9.5 55.0 1.9 56.0 2.2 57.0 9.8 58.0 37.1 59.0 2.3 70.0 2.1 71.0 1.0 84.0 1.2 86.0 100.0 87.0 6.2 101.0 3.1
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C6 H15 N 0.05 ml : 0.5 ml CDCl3 N-ethyl-tert-butylamine Assign. Shift(ppm)
A 2.603 B 1.104 C 1.099 D 1.
Hz ppm Int.
1051.27 2.631 100 1044.07 2.613 271 1036.99 2.595 278 1029.91 2.578 109 446.66 1.118 358 441.16 1.104 1000 439.21 1.099 700 432.13 1.082 334 378.30 0.947 21
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1H NMR 89.56 MHz C6 H15 N 0.04 ml : 0.5 ml CDCl3 N-ethyl-tert-butylamine Assign. Shift(ppm)
A 2.60 B 1.101 C 1.101 D 0.76
Hz ppm Int.
236.63 2.643 53 229.56 2.564 59 105.06 1.174 68 100.56 1.123 28 98.63 1.102 1000 90.88 1.015 50
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