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MassMS-IW-9711 5-benzyl-3-phenyl-2-thioxo-4-imidazolidone C16H14N2OS (Mass of molecular ion: 282)
Source Temperature: 160 °C Sample Temperature: 140 °C Direct, 75 eV
28.0 4.0 39.0 1.9 50.0 1.1 51.0 4.5 59.0 1.3 63.0 1.2 65.0 4.4 76.0 1.1 77.0 13.6 78.0 3.1 89.0 1.1 90.0 1.2 91.0 100.0 92.0 9.5 93.0 1.0 103.0 3.1 104.0 3.6 109.0 1.5 117.0 1.3 118.0 1.4 119.0 1.3 128.0 1.3 131.0 1.2 135.0 6.9 136.0 10.3 137.0 1.2 191.0 5.5 204.0 1.1 249.0 3.2 253.0 1.1 282.0 28.9 283.0 5.5 284.0 1.8
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C16 H14 N2 O S 0.034 g : 0.5 ml DMSO-d6 5-benzyl-3-phenyl-2-thioxo-4-imidazolidone 
Assign. Shift(ppm)
A 10.6 B 7.37 C 7.31 D 7.21 E 6.782 F 4.769 G 3.125
Hz ppm Int.4247.26 10.628 343 2960.89 7.409 114 2959.24 7.405 70 2957.41 7.401 177 2955.76 7.396 107 2954.11 7.392 108 2951.91 7.387 495 2948.06 7.377 263 2947.15 7.375 393 2944.77 7.369 1000 2943.12 7.365 417 2942.20 7.362 244 2939.64 7.356 203 2938.17 7.352 160 2934.69 7.344 104 2933.05 7.340 120 2931.03 7.334 157 2929.38 7.330 113 2928.28 7.328 99 2925.72 7.321 432 2924.99 7.319 365 2924.07 7.317 289 2921.69 7.311 379 2920.59 7.308 435 2918.57 7.303 872 2917.48 7.301 503 2914.18 7.292 210 2912.90 7.289 162 2907.95 7.277 62 2906.30 7.273 51 2892.02 7.237 41 2887.80 7.226 534 2885.42 7.220 416 2883.59 7.216 215 2882.86 7.214 212 2881.94 7.212 226 2880.11 7.207 412 2878.46 7.203 342 2875.53 7.196 53 2715.99 6.796 477 2713.79 6.791 399 2711.96 6.786 191 2707.93 6.776 499 2706.28 6.772 442 2702.99 6.764 64 1910.24 4.780 150 1906.58 4.771 328 1905.66 4.769 325 1901.82 4.759 155 1251.21 3.131 578 1246.81 3.120 553
in DMSO-d6
KBr disc
nujol mull
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