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4-Nitro-N-methylphthalimide

Product Name 4-Nitro-N-methylphthalimide

CAS41663-84-7

MFC9H6N2O4

MW206.15

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  • Mass 

    MS-KW-0586          
N-methyl-4-nitrophthalimide
C9H6N2O4            (Mass of molecular ion:    206)


       Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV


          28.0       3.3
      30.0       1.9
      37.0       1.3
      38.0       1.0
      50.0       1.6
      51.0       1.4
      51.5       1.4
      53.0       1.1
      62.0       1.7
      63.0       3.0
      65.0       1.0
      73.0       1.7
      74.0      12.1
      75.0      42.4
      76.0       5.7
      77.0       3.5
      89.0       1.1
     103.0      56.2
     104.0       8.5
     105.0       1.0
     116.0       9.6
     117.0       1.1
     119.0       2.0
     120.0       2.3
     131.0       5.0
     132.0      15.1
     133.0       1.5
     149.0       8.8
     150.0       2.8
     159.0       6.4
     160.0       5.2
     161.0       2.5
     162.0       4.8
     178.0       1.6
     205.0       6.5
     206.0     100.0
     207.0      10.8
     208.0       1.4

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9H6N2O4 0.038 g : 0.5 ml CDCl3
    N-methyl-4-nitrophthalimide
    ChemicalStructure 
        Assign.     Shift(ppm)
    
     A           8.658
     B           8.622
     C           8.076
     D           3.263
  

         Hz     ppm     Int.


       3462.65   8.662    126
   3462.04   8.660    132
   3460.58   8.657    165
   3459.97   8.655    147
   3451.54   8.634    131
   3449.59   8.629     93
   3443.49   8.614    131
   3441.53   8.609    105
   3232.55   8.086    144
   3231.94   8.085    137
   3224.49   8.066    136
   3223.88   8.065    128
   1304.33   3.263   1000

in CDCl3



KBr disk



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