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41105-36-6More Spectrum > 2-CHLORO-9,10-BIS(PHENYLETHYNYL)ANTHRACENE(41105-36-6)IR1
2-CHLORO-9,10-BIS(PHENYLETHYNYL)ANTHRACENE
Product Name 2-CHLORO-9,10-BIS(PHENYLETHYNYL)ANTHRACENE
CAS41105-36-6
MFC30H17Cl
MW412.91
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MS-NW-8027 2-chloro-9,10-bis(phenylethynyl)anthracene C30H17Cl (Mass of molecular ion: 412)
Source Temperature: 220 °C Sample Temperature: 210 °C Direct, 75 eV
18.0 1.2 148.0 1.0 149.0 1.2 161.0 2.1 162.0 1.9 167.5 1.2 173.0 1.5 174.0 2.8 175.0 2.1 186.0 2.3 186.5 1.1 187.0 6.9 187.5 3.1 188.0 2.5 206.0 10.3 206.5 3.6 207.0 3.8 207.5 1.1 298.0 2.1 299.0 1.1 300.0 3.6 322.0 1.3 335.0 1.0 346.0 1.2 348.0 2.0 350.0 1.8 372.0 3.8 373.0 2.1 374.0 13.0 375.0 6.1 376.0 10.7 377.0 3.7 378.0 1.0 410.0 2.2 411.0 1.5 412.0 100.0 413.0 33.4 414.0 37.5 415.0 11.6 416.0 1.8
400 MHz at 65C
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1H NMR 399.65 MHz C30 H17 Cl 0.034 g : 0.5 ml CDCl3 at 65 C 2-chloro-9,10-bis(phenylethynyl)anthracene Assign. Shift(ppm)
A 8.57 B 8.56 C 8.518 D 7.72 E 7.57 F 7.465 G 7.43 to 7.40
Hz ppm Int.
3433.35 8.591 58 3431.27 8.586 351 3428.71 8.580 179 3426.39 8.574 213 3425.78 8.572 214 3421.63 8.562 645 3420.04 8.558 463 3408.81 8.530 303 3399.66 8.507 314 3095.21 7.745 329 3093.51 7.741 298 3091.55 7.736 162 3088.50 7.729 532 3087.40 7.726 582 3085.94 7.722 648 3083.25 7.715 205 3082.40 7.713 228 3080.69 7.709 425 3079.10 7.705 391 3076.42 7.698 65 3036.50 7.598 54 3031.86 7.587 322 3029.79 7.582 176 3027.59 7.576 185 3026.98 7.575 194 3026.12 7.572 196 3024.41 7.568 167 3024.05 7.567 168 3021.97 7.562 328 3017.33 7.550 51 2989.14 7.480 220 2987.06 7.475 223 2979.98 7.457 221 2978.03 7.452 299 2975.22 7.445 199 2973.63 7.441 133 2971.80 7.437 190 2968.87 7.429 458 2965.82 7.422 474 2963.75 7.416 469 2961.67 7.411 1000 2959.11 7.405 787 2955.93 7.397 237 2954.35 7.393 211 2952.64 7.389 133 2950.20 7.382 49 2949.46 7.381 55 2947.63 7.376 78 2945.92 7.372 54
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