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1,10-Dibromodecane

Product Name 1,10-Dibromodecane

CAS4101-68-2

MFC10H20Br2

MW300.07

¹³CNMR

Mass

MS-NW-2751          
1,10-dibromodecane
C10H20Br2           (Mass of molecular ion:    298)

   Source Temperature: 290 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      18.0       1.0
      27.0      17.7
      28.0       1.9
      29.0      18.1
      39.0      13.1
      40.0       2.4
      41.0      62.7
      42.0      10.9
      43.0      47.9
      44.0       1.6
      53.0       5.3
      54.0       4.9
      55.0     100.0
      56.0      11.0
      57.0      51.3
      58.0       2.3
      67.0       8.1
      68.0       5.6
      69.0      66.0
      70.0       6.2
      71.0      40.9
      72.0       2.3
      80.0       2.4
      81.0       4.7
      82.0       2.9
      83.0      48.1
      84.0       4.0
      85.0      14.4
      86.0       1.0
      93.0       1.1
      95.0       2.9
      96.0       1.3
      97.0      25.0
      98.0       1.9
     107.0       5.9
     109.0       5.7
     121.0       3.5
     123.0       3.2
     135.0      43.6
     136.0       2.8
     137.0      42.9
     138.0       1.9
     139.0       3.6
     149.0       3.4
     150.0      10.0
     151.0       3.9
     152.0       9.4
     162.0       1.0
     163.0      10.2
     164.0       1.6
     165.0      10.3
     177.0       6.7
     179.0       6.6
     219.0       4.0
     221.0       3.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₂₀ Br₂	0.04 ml : 0.5 ml CDCl₃
1,10-dibromodecane

    Assign.     Shift(ppm)

      A             3.398
      B             1.86
      C             1.50
      D             1.31

     Hz     ppm     Int.

    311.69   3.481    320
    304.94   3.405    841
    298.06   3.329    465
    176.50   1.971     31
    174.06   1.944     72
    172.81   1.930     84
    172.31   1.924     82
    170.19   1.901     67
    169.44   1.892     70
    166.44   1.859    133
    165.56   1.849    131
    162.44   1.814     71
    159.38   1.780    120
    155.81   1.740     49
    155.19   1.733     41
    153.81   1.718     47
    153.31   1.712     46
    141.00   1.575     32
    140.56   1.570     33
    140.13   1.565     34
    139.75   1.561     36
    139.06   1.553     35
    138.63   1.548     36
    138.38   1.546     36
    137.81   1.539     38
    133.94   1.496     79
    132.88   1.484     78
    132.50   1.480     81
    132.13   1.476     81
    129.88   1.451    106
    128.69   1.437    100
    127.88   1.428    104
    125.88   1.406    155
    125.13   1.398    153
    117.50   1.312   1000
    109.81   1.227     60

in CDCl3

KBr disc

liquid film

nujol mull

4880 A,200 M,powder

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