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4081-35-0

N,N'-BIS(SALICYLIDENE)-1,6-HEXANEDIAMINE

Product Name N,N'-BIS(SALICYLIDENE)-1,6-HEXANEDIAMINE

CAS4081-35-0

MFC20H24N2O2

MW324.42

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  • 4081-35-0_ms_1
    Mass 

    MS-NW-7047          
N,N'-disalicylidene-1,6-hexanediamine
C20H24N2O2          (Mass of molecular ion:    324)


       Source Temperature: 180 °C
   Sample Temperature: 130 °C
   Direct, 75 eV


          18.0       1.1
      27.0       3.4
      28.0       7.6
      29.0       3.8
      30.0       3.2
      39.0       8.6
      40.0       1.2
      41.0      17.8
      42.0       3.1
      43.0       2.7
      44.0       1.6
      50.0       1.5
      51.0       8.5
      52.0       2.8
      53.0       3.3
      54.0       2.7
      55.0       9.7
      56.0       4.7
      57.0       1.1
      63.0       2.0
      64.0       1.7
      65.0       9.0
      66.0       4.2
      67.0       3.1
      68.0       1.7
      69.0       3.3
      70.0       3.4
      76.0       1.7
      77.0      22.5
      78.0       9.5
      79.0       7.8
      80.0       1.9
      81.0       2.0
      82.0       4.1
      83.0       3.3
      84.0       7.6
      89.0       1.0
      90.0       1.2
      91.0       5.4
      92.0       2.7
      93.0       7.9
      94.0       2.4
      95.0       4.4
      96.0       8.5
      97.0       3.5
      98.0       2.0
     102.0       4.0
     103.0       2.7
     104.0       3.0
     105.0       5.5
     106.0       4.3
     107.0      49.1
     108.0       5.2
     116.0       1.6
     117.0       2.3
     118.0       6.0
     119.0       3.9
     120.0      21.1
     121.0      22.6
     122.0      21.8
     123.0       3.1
     130.0       1.1
     131.0       6.0
     132.0       6.9
     133.0       6.6
     134.0      24.4
     135.0      19.1
     136.0       6.7
     145.0       1.0
     146.0       4.6
     147.0       3.9
     148.0      60.3
     149.0      17.9
     150.0       2.3
     158.0       1.1
     160.0       6.7
     161.0       2.5
     162.0      27.9
     163.0       6.3
     172.0       1.0
     174.0       6.3
     175.0       5.3
     176.0      15.7
     177.0       4.7
     186.0      14.1
     187.0       2.4
     188.0       8.4
     189.0       3.8
     190.0      11.9
     191.0       1.7
     200.0       2.3
     201.0       2.1
     202.0      74.4
     203.0     100.0
     204.0      24.1
     205.0      28.0
     206.0       4.5
     217.0       3.6
     227.0       1.0
     324.0      36.7
     325.0       8.7
     326.0       1.4

400 MHz in CDCl3

  • 4081-35-0_1hnmr_0

    1H NMR 399.65 MHz
    C20 H24 N2 O2 0.038 g : 0.5 ml CDCl3
    N,N'-disalicylidene-1,6-hexanediamine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A            13.6
      B             8.313
      C             7.285
      D             7.224
      E             6.949
      F             6.855
      G             3.572
      J             1.699
      K             1.426
  

         Hz     ppm     Int.


       5456.89  13.655     89
   3322.46   8.314    992
   2920.96   7.309    258
   2919.12   7.305    294
   2913.63   7.291    332
   2912.53   7.288    429
   2911.98   7.287    455
   2910.88   7.284    407
   2905.39   7.270    319
   2903.56   7.266    370
   2892.02   7.237    484
   2890.37   7.233    457
   2884.32   7.218    553
   2882.67   7.213    495
   2781.20   6.960    607
   2773.87   6.941    518
   2773.32   6.940    540
   2772.96   6.939    540
   2747.31   6.875    386
   2746.22   6.872    386
   2739.80   6.856    597
   2738.89   6.854    611
   2735.23   6.845     38
   2732.29   6.837    327
   2731.38   6.835    323
   1435.11   3.591    457
   1434.01   3.589    487
   1428.33   3.574    963
   1427.23   3.572   1000
   1421.56   3.558    498
   1420.46   3.555    508
    685.96   1.717    283
    679.18   1.700    440
    674.60   1.688    253
    672.04   1.682    322
    666.36   1.668    106
    665.26   1.665    107
    577.34   1.445    316
    573.86   1.436    390
    570.01   1.427    687
    566.35   1.418    377
    562.69   1.408    261

in CDCl3

KBr disc

nujol mull

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