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MS-IW-0070 2,5-dimethylbenzophenone C15H14O (Mass of molecular ion: 210)
Source Temperature: 250 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.9 39.0 2.5 50.0 1.6 51.0 7.5 52.0 1.0 53.0 1.4 63.0 2.0 65.0 2.0 76.0 2.1 77.0 36.0 78.0 4.6 79.0 9.0 82.0 1.0 89.0 2.5 90.0 1.0 91.0 2.7 96.0 1.0 97.0 1.9 103.0 6.3 104.0 4.7 105.0 39.9 106.0 3.3 119.0 6.6 133.0 22.9 134.0 2.3 152.0 1.8 165.0 7.2 166.0 3.1 167.0 1.9 177.0 1.5 178.0 4.6 179.0 1.4 181.0 2.2 191.0 4.1 192.0 6.4 193.0 6.0 194.0 24.6 195.0 26.1 196.0 7.0 208.0 2.1 209.0 100.0 210.0 72.0 211.0 10.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H14 O 0.05 ml : 0.5 ml CDCl3 2,5-dimethylbenzophenone Assign. Shift(ppm)
A 7.798 B 7.536 C 7.419 D 7.170 E 7.148 F 7.108 G *1 2.303 J *1 2.257
Hz ppm Int.
3120.73 7.809 315 3120.12 7.808 278 3119.51 7.806 384 3118.29 7.803 167 3117.80 7.802 141 3114.38 7.793 123 3112.43 7.788 429 3111.08 7.785 383 3021.61 7.561 59 3020.26 7.558 112 3018.92 7.554 65 3014.89 7.544 78 3012.94 7.539 236 3010.99 7.535 92 3006.84 7.524 116 3005.49 7.521 201 3004.15 7.517 109 2974.00 7.442 79 2972.90 7.439 271 2972.41 7.438 319 2970.83 7.434 143 2965.58 7.421 257 2964.48 7.418 398 2963.26 7.415 142 2958.86 7.404 91 2957.15 7.400 216 2956.54 7.398 154 2955.57 7.396 65 2872.68 7.188 58 2871.22 7.185 62 2864.87 7.169 200 2863.40 7.165 228 2858.76 7.154 340 2850.95 7.134 100 2840.94 7.109 246 920.41 2.304 968 919.92 2.302 942 902.22 2.258 1000