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MassMS-IW-9602 3beta-acetoxy-14,15beta-epoxy-5beta,14beta-bufa-20,22-dienolide C26H34O5 (Mass of molecular ion: 426)
Source Temperature: 190 °C Sample Temperature: 200 °C Direct, 75 eV
17.0 15.5 18.0 70.9 26.0 2.3 27.0 11.9 28.0 27.8 29.0 19.2 31.0 1.6 38.0 1.1 39.0 19.9 40.0 5.1 41.0 67.8 42.0 3.9 43.0 35.1 44.0 7.2 45.0 1.6 50.0 2.6 51.0 8.2 52.0 4.2 53.0 30.7 54.0 7.0 55.0 64.1 56.0 4.2 57.0 11.2 58.0 1.1 62.0 1.0 63.0 3.7 64.0 2.6 65.0 20.7 66.0 16.5 67.0 55.7 68.0 9.6 69.0 29.9 70.0 3.3 71.0 5.0 72.0 2.4 74.0 1.0 75.0 1.4 76.0 2.1 77.0 48.9 78.0 15.1 79.0 82.8 80.0 15.5 81.0 66.2 82.0 10.1 82.5 1.1 83.0 13.9 84.0 6.9 85.0 24.7 86.0 2.6 87.0 1.2 88.0 1.4 89.0 5.1 90.0 2.9 91.0 100.0 92.0 23.3 93.0 78.1 94.0 43.7 94.5 1.0 95.0 65.5 96.0 10.4 97.0 10.9 98.0 4.7 99.0 3.4 100.0 1.9 101.0 2.7 102.0 2.9 103.0 9.6 104.0 7.7 105.0 84.5 105.5 1.2 106.0 39.0 106.5 1.4 107.0 92.9 107.5 1.0 108.0 54.5 109.0 66.4 110.0 24.5 111.0 11.2 112.0 3.6 113.0 3.2 114.0 2.5 115.0 20.8 116.0 10.1 117.0 30.8 118.0 26.6 119.0 54.5 120.0 32.5 121.0 50.3 122.0 62.8 123.0 66.8 124.0 14.1 125.0 6.1 126.0 3.7 126.5 1.2 127.0 7.2 128.0 18.9 129.0 26.6 130.0 11.6 131.0 45.5 132.0 18.6 133.0 50.4 134.0 26.8 135.0 31.4 136.0 25.4 137.0 20.1 138.0 19.4 139.0 5.8 140.0 5.4 141.0 15.6 142.0 11.5 143.0 27.7 144.0 18.2 145.0 50.6 146.0 20.4 147.0 54.9 148.0 19.8 149.0 18.4 150.0 6.5 151.0 5.0 152.0 6.7 153.0 8.5 154.0 5.9 155.0 14.0 156.0 10.6 157.0 25.4 158.0 17.6 159.0 40.5 160.0 29.8 161.0 35.3 162.0 21.3 163.0 10.5 164.0 5.7 165.0 12.1 166.0 7.2 167.0 9.0 168.0 5.9 169.0 15.5 170.0 8.8 171.0 22.8 172.0 13.0 173.0 24.3 174.0 20.8 175.0 22.4 176.0 11.3 177.0 9.7 178.0 11.5 179.0 7.6 180.0 5.7 181.0 10.4 182.0 6.1 183.0 15.4 184.0 7.5 185.0 21.7 186.0 10.5 187.0 22.3 188.0 35.2 189.0 18.7 190.0 11.2 191.0 17.3 192.0 6.1 193.0 7.0 194.0 5.5 195.0 10.4 196.0 7.1 197.0 16.0 198.0 8.1 199.0 23.6 200.0 12.4 201.0 20.2 202.0 9.9 203.0 30.2 204.0 8.4 205.0 7.4 206.0 5.1 207.0 19.0 208.0 5.4 209.0 9.8 210.0 5.5 211.0 15.5 212.0 8.6 213.0 43.6 214.0 76.5 215.0 42.0 216.0 19.4 217.0 10.2 218.0 4.3 219.0 5.4 220.0 2.6 221.0 4.4 222.0 2.9 223.0 7.8 224.0 4.9 225.0 13.4 226.0 9.5 227.0 15.7 228.0 25.4 229.0 17.0 230.0 8.9 231.0 16.6 232.0 27.7 233.0 8.8 234.0 3.2 235.0 4.4 236.0 3.0 237.0 4.9 238.0 4.0 239.0 8.3 240.0 7.5 241.0 17.5 242.0 11.7 243.0 10.9 244.0 5.9 245.0 8.2 246.0 8.7 247.0 4.1 248.0 3.1 249.0 7.5 250.0 10.4 251.0 6.0 252.0 5.0 253.0 6.0 254.0 7.1 255.0 6.8 256.0 6.5 257.0 7.5 258.0 3.6 259.0 3.3 260.0 1.7 261.0 1.8 263.0 2.2 264.0 1.7 265.0 2.9 266.0 1.4 267.0 4.5 268.0 4.3 269.0 3.4 270.0 2.4 271.0 1.7 272.0 1.3 273.0 1.5 275.0 2.0 276.0 1.1 277.0 2.8 278.0 2.1 279.0 3.5 280.0 2.4 281.0 4.1 282.0 2.2 283.0 1.8 284.0 1.0 289.0 2.4 290.0 1.9 291.0 2.3 292.0 1.3 293.0 3.6 294.0 2.9 295.0 6.5 296.0 20.4 297.0 5.1 298.0 3.0 299.0 1.5 303.0 1.0 304.0 1.9 305.0 2.3 306.0 2.4 307.0 5.5 308.0 4.7 309.0 4.1 310.0 1.6 311.0 1.4 314.0 1.3 317.0 2.1 318.0 1.0 321.0 3.5 322.0 6.4 323.0 2.3 324.0 2.1 325.0 37.8 326.0 10.2 327.0 1.7 332.0 2.0 333.0 1.5 335.0 24.1 336.0 6.6 337.0 1.2 339.0 1.0 340.0 1.9 341.0 1.1 343.0 3.0 344.0 1.0 348.0 1.3 350.0 65.6 351.0 18.2 352.0 3.3 353.0 4.0 354.0 1.0 368.0 17.7 369.0 4.9 386.0 2.8 387.0 1.1
KBr disc
nujol mull
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