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4-Amino-3-nitrobenzotrifluoride

Product Name 4-Amino-3-nitrobenzotrifluoride

CAS400-98-6

MFC7H5F3N2O2

MW206.12

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  • Mass

    MS-IW-0061          
    2-nitro-4-(trifluoromethyl)aniline
    C7H5F3N2O2          (Mass of molecular ion:    206)
    

       Source Temperature: 240 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          18.0       1.6
          28.0       3.6
          30.0       3.4
          37.0       1.0
          38.0       1.9
          39.0       2.2
          41.0       1.4
          50.0       1.5
          51.0       2.3
          52.0       6.0
          53.0       1.1
          57.0       2.1
          61.0       1.2
          62.0       2.7
          63.0       8.4
          64.0       3.4
          65.0       2.5
          69.0       2.9
          75.0       2.9
          76.0       1.4
          78.0       1.5
          81.0       1.3
          82.0       1.0
          83.0       5.2
          88.0       1.7
          89.0       1.6
          90.0       2.2
          91.0       2.6
          95.0       2.3
          98.0       1.5
         100.0       1.0
         101.0       2.3
         107.0       1.0
         108.0       1.1
         109.0       1.3
         110.0       2.6
         113.0      17.9
         114.0       3.4
         120.0      11.3
         121.0       1.2
         127.0       1.1
         128.0       1.7
         132.0       3.4
         133.0      11.0
         134.0       1.0
         139.0       2.1
         140.0      24.0
         141.0       6.0
         143.0       1.7
         145.0       1.1
         148.0      11.6
         158.0       1.5
         159.0       3.7
         160.0      61.6
         161.0       4.9
         176.0      10.4
         187.0       8.5
         189.0       4.3
         190.0       2.6
         206.0     100.0
         207.0       9.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H5 F3 N2 O2 0.041 g : 0.5 ml CDCl3
    2-nitro-4-(trifluoromethyl)aniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.421 B 7.556 C 6.933 D 6.43

         Hz     ppm     Int.
    

       3366.46   8.424    992
       3365.48   8.422   1000
       3025.27   7.570    598
       3023.19   7.565    595
       3016.48   7.548    640
       3014.40   7.543    637
       3010.38   7.533     30
       2775.15   6.944    922
       2766.36   6.922    862
       2569.09   6.429    206
    

in CDCl3



KBr disc



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