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39968-33-7

HOAt

Product Name HOAt

CAS39968-33-7

MFC5H4N4O

MW136.11

More

  • 39968-33-7_ms
    Mass

    MS-IW-9314          
    3H-1,2,3-triazolo(4,5-b)pyridin-3-ol
    C5H4N4O             (Mass of molecular ion:    136)
    

       Source Temperature: 160 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          17.0       1.4
          18.0       5.5
          25.0       1.1
          26.0       8.9
          27.0       6.1
          28.0      32.6
          29.0       1.8
          30.0       9.1
          36.0       2.0
          37.0      21.6
          38.0      31.6
          39.0      22.7
          40.0      18.5
          41.0       5.1
          44.0       2.8
          45.0       1.4
          49.0       3.4
          50.0      14.3
          51.0      29.9
          52.0      28.2
          53.0      38.3
          54.0       4.0
          55.0       1.5
          62.0       2.6
          63.0       8.2
          64.0      38.1
          65.0      13.4
          66.0       2.7
          67.0       1.0
          75.0       2.4
          76.0       4.8
          77.0       5.0
          78.0     100.0
          79.0      14.0
          80.0       2.3
          91.0      40.8
          92.0      17.4
          93.0       1.2
          94.0       1.2
         108.0      85.5
         109.0       5.6
         120.0       7.9
         137.0       2.1
    

400 MHz in DMSO-d6

  • 39968-33-7_1hnmr

    1H NMR 399.65 MHz
    C5 H4 N4 O 0.038 g : 0.5 ml DMSO-d6
    3H-1,2,3-triazolo(4,5-b)pyridin-3-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.825 B 8.588 C 7.566

         Hz     ppm     Int.
    

       3535.40   8.847     38
       3529.66   8.832    893
       3528.32   8.829    852
       3525.27   8.821    899
       3523.93   8.818    791
       3437.38   8.601    969
       3436.04   8.598    945
       3428.96   8.580   1000
       3427.61   8.577    940
       3030.03   7.582    947
       3025.63   7.571    915
       3021.61   7.561    909
       3017.21   7.550    878
    

in DMSO-d6

  • 39968-33-7_13cnmr

KBr disc

  • 39968-33-7_ir1_2

nujol mull

  • 39968-33-7_ir2