2-Amino-5-fluorobenzotrifluoride

Mass

MS-IW-2189          
4-fluoro-2-(trifluoromethyl)aniline
C7H5F4N             (Mass of molecular ion:    179)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      28.0       2.9
      31.0       2.9
      37.0       1.0
      38.0       1.2
      39.0       1.3
      46.0       1.2
      50.0       1.6
      51.0       1.7
      52.0       3.2
      54.5       2.2
      56.0       2.1
      57.0       5.5
      61.0       1.6
      62.0       2.2
      63.0       7.3
      64.0       1.3
      66.0       1.5
      69.0       2.7
      70.0       1.2
      75.0       4.0
      79.5       5.7
      80.0       3.7
      81.0       6.0
      82.0       4.0
      83.0       5.1
      88.0       2.4
      89.0       1.3
      89.5       1.9
      90.0       1.4
      94.0       2.8
      95.0       1.4
      99.0       1.2
     101.0       6.3
     106.0       1.3
     108.0       2.4
     109.0       5.3
     110.0       1.0
     112.0       1.5
     113.0       2.9
     120.0       3.0
     129.0       2.3
     131.0       1.9
     132.0     100.0
     133.0       7.1
     138.0       2.1
     139.0       1.8
     140.0       5.4
     151.0       4.2
     158.0       3.9
     159.0      63.3
     160.0      20.8
     161.0       1.5
     178.0       4.8
     179.0      87.0
     180.0       7.0

Parameter ppm Hz D(A) 7.10 D(B) 6.96 D(C) 6.59 J(A,B) 2.98 J(A,C) 0.23 J(A,X) 8.65 J(A,Y) -0.54 J(B,C) 8.92 J(B,X) 7.68 J(B,Y) -0.70 J(C,X) 4.42 J(C,Y) 0.75 J(X,Y) 0.0 D(D) 3.94 AKSNES,D. & KRONHAUG,F.H. ACTA CHEM.SCAND. 25, 1871 (1971)

     Hz     ppm     Int.

   2135.87   7.120     73
   2132.87   7.110     76
   2127.03   7.090     69
   2124.39   7.081     74
   2098.11   6.994     34
   2097.57   6.992     34
   2095.14   6.984     34
   2094.61   6.982     31
   2090.57   6.969     36
   2089.95   6.966     46
   2089.21   6.964     51
   2088.61   6.962     50
   2087.73   6.959     45
   2086.95   6.956     48
   2086.27   6.954     49
   2081.67   6.939     38
   2080.99   6.937     38
   2078.71   6.929     34
   2078.05   6.927     33
   1983.43   6.611     65
   1979.45   6.598     64
   1978.77   6.596     65
   1974.50   6.582     63
   1970.47   6.568     55
   1969.81   6.566     55
   1181.99   3.940   1000