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MassMS-IW-4070 2,3,4-trifluoroaniline C6H4F3N (Mass of molecular ion: 147)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 4.2 31.0 3.3 50.0 2.4 51.0 4.2 52.0 2.1 56.0 1.4 57.0 1.8 68.0 1.4 69.0 4.0 70.0 6.7 73.5 6.2 74.0 1.4 75.0 4.2 76.0 2.5 77.0 1.2 80.0 1.7 81.0 2.8 91.0 1.6 92.0 1.1 93.0 2.3 94.0 1.5 96.0 1.0 99.0 5.8 100.0 12.3 101.0 6.1 107.0 3.0 108.0 1.5 116.0 2.7 119.0 20.4 120.0 26.0 121.0 1.9 126.0 3.5 127.0 7.5 128.0 1.4 130.0 1.1 146.0 5.7 147.0 100.0 148.0 7.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H4 F3 N 0.05 ml : 0.5 ml CDCl3 2,3,4-trifluoroaniline 
Assign. Shift(ppm)
A 6.750 B 6.439 C 3.71
Hz ppm Int.2712.65 6.788 455 2710.33 6.782 446 2704.83 6.768 496 2703.37 6.765 702 2702.64 6.763 891 2701.05 6.759 691 2700.44 6.758 583 2695.56 6.745 654 2694.95 6.744 601 2693.48 6.740 1000 2691.16 6.734 594 2685.67 6.721 519 2683.35 6.715 521 2585.94 6.471 500 2583.37 6.465 528 2581.05 6.459 532 2578.61 6.453 547 2576.90 6.448 893 2574.34 6.442 902 2572.14 6.436 878 2569.58 6.430 894 2567.75 6.425 504 2565.19 6.419 477 2562.99 6.414 454 2560.42 6.407 452 1482.18 3.709 590
liquid film
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