3-(Perfluoro-n-octyl)propenoxide

Mass

MS-IW-7441          
2-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononyl)oxirane
C11H5F17O           (Mass of molecular ion:    476)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       4.8
      27.0       8.1
      28.0       4.4
      29.0      36.2
      30.0       1.4
      31.0      26.3
      33.0       2.3
      39.0       2.4
      41.0       4.8
      42.0       2.3
      43.0      45.3
      44.0       1.9
      47.0       2.8
      51.0      17.5
      55.0       1.8
      57.0      91.7
      58.0       3.9
      59.0      19.9
      61.0       2.6
      64.0       1.8
      65.0       4.7
      69.0      45.7
      71.0       2.0
      75.0       2.4
      76.0       1.5
      77.0      21.0
      78.0       1.2
      79.0       7.0
      81.0       1.0
      87.0       1.3
      88.0       1.3
      89.0       3.3
      90.0       1.1
      91.0       5.5
      93.0       1.6
      95.0       8.7
     100.0       7.0
     101.0       1.2
     105.0       1.0
     107.0     100.0
     108.0       6.0
     109.0      15.4
     113.0       1.8
     115.0       1.2
     119.0      15.6
     120.0       1.1
     121.0       1.0
     122.0       1.1
     127.0       2.4
     131.0      14.9
     133.0       1.2
     139.0       2.9
     145.0       1.5
     157.0       1.1
     169.0       7.3
     170.0       1.4
     181.0       2.9
     231.0       1.8
     339.0       1.6
     345.0       1.6
     363.0       1.4
     389.0       1.8
     428.0       1.1
     437.0       1.2
     441.0       3.3
     461.0       2.3
     476.0      22.0
     477.0       2.7

Assign. Shift(ppm) A 3.223 B 2.878 C 2.582 D *1 2.416 E *1 2.254

     Hz     ppm     Int.

   1297.24   3.246    148
   1294.80   3.240    185
   1293.46   3.237    219
   1291.26   3.231    391
   1288.70   3.225    373
   1288.09   3.224    386
   1285.52   3.217    403
   1283.45   3.212    236
   1282.10   3.209    218
   1279.54   3.202    176
   1154.79   2.890    656
   1154.42   2.889    666
   1150.27   2.879   1000
   1146.12   2.868    701
   1145.63   2.867    680
   1035.77   2.592    784
   1033.33   2.586    808
   1031.01   2.580    770
   1028.44   2.574    739
    995.97   2.493     58
    989.99   2.478     55
    978.52   2.449    158
    976.68   2.444    121
    972.53   2.434    150
    963.01   2.410    191
    957.03   2.395    192
    945.19   2.366    102
    939.21   2.351     95
    928.10   2.323     99
    922.73   2.309     96
    909.79   2.277    212
    908.08   2.273    169
    904.42   2.264    195
    894.65   2.239    145
    892.94   2.235    142
    891.60   2.231    153
    889.53   2.226    175
    887.70   2.222    137
    886.47   2.219    129
    876.46   2.194     70
    875.00   2.190     46
    871.09   2.180     66
    869.63   2.176     42