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MS-NW-7473 (-)-cis-myrtanylamine C10H19N (Mass of molecular ion: 153)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
27.0 2.7 28.0 1.7 29.0 1.9 30.0 100.0 31.0 1.7 39.0 3.9 41.0 9.7 42.0 1.3 43.0 3.6 53.0 2.5 54.0 3.2 55.0 3.6 56.0 4.0 57.0 1.0 58.0 1.5 65.0 1.0 67.0 8.3 68.0 2.5 69.0 6.8 70.0 2.6 71.0 5.5 77.0 1.8 79.0 3.9 80.0 1.7 81.0 6.0 82.0 4.3 83.0 1.1 84.0 2.1 91.0 1.4 93.0 4.0 94.0 1.3 95.0 1.5 96.0 1.2 107.0 1.5 110.0 3.1 121.0 1.6 123.0 1.3 124.0 1.2 136.0 1.0 138.0 3.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H19 N 0.05 ml : 0.5 ml CDCl3 (-)-cis-myrtanylamine Assign. Shift(ppm)
A 2.66 B 2.359 C 2.00 to 1.88 D 1.61 E 1.443 F 1.185 G 0.973 J 0.905
Hz ppm Int.
1068.85 2.675 138 1061.89 2.658 212 1054.93 2.640 121 949.22 2.376 59 947.39 2.371 54 946.41 2.369 61 943.24 2.361 57 941.16 2.355 52 939.82 2.352 65 937.99 2.348 55 809.20 2.025 56 807.50 2.021 59 802.25 2.008 58 800.78 2.004 70 799.80 2.002 73 796.39 1.993 70 793.46 1.986 86 791.63 1.981 73 788.45 1.973 130 787.11 1.970 174 785.28 1.965 111 781.98 1.957 105 779.30 1.950 117 777.10 1.945 124 775.39 1.941 113 774.41 1.938 109 771.97 1.932 84 766.72 1.919 135 765.38 1.916 143 763.31 1.910 176 760.50 1.903 139 757.93 1.897 125 755.37 1.891 83 753.78 1.887 87 752.56 1.884 83 749.27 1.875 51 747.19 1.870 67 744.63 1.864 53 741.46 1.856 55 643.92 1.612 75 588.75 1.474 49 582.40 1.458 60 578.00 1.447 51 574.46 1.438 58 473.88 1.186 1000 388.92 0.974 987 366.58 0.918 206 357.06 0.894 200
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