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MassMS-NW-8942 3-(bromomethyl)pentane C6H13Br (Mass of molecular ion: 164)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 11.5 28.0 2.5 29.0 16.0 39.0 9.6 40.0 1.3 41.0 25.0 42.0 5.7 43.0 93.0 44.0 3.2 51.0 1.0 53.0 3.9 54.0 1.2 55.0 59.2 56.0 14.6 57.0 11.0 69.0 9.3 70.0 7.2 71.0 31.9 72.0 1.8 84.0 1.8 85.0 100.0 86.0 6.7 107.0 2.3 109.0 2.1 135.0 7.5 137.0 7.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H13 Br 0.05 ml : 0.5 ml CDCl3 3-(bromomethyl)pentane 
Assign. Shift(ppm)
A 3.460 B 1.45 C 1.427 D 0.895
Hz ppm Int.1393.92 3.488 22 1385.13 3.466 485 1380.62 3.455 482 573.97 1.437 440 566.65 1.418 431 560.79 1.404 231 559.81 1.401 242 384.28 0.962 28 383.91 0.961 28 382.45 0.957 25 381.96 0.956 25 381.35 0.955 26 377.56 0.945 40 377.20 0.944 40 376.83 0.943 40 364.38 0.912 651 357.18 0.894 1000 349.61 0.875 494 343.51 0.860 39 340.33 0.852 21
in CDCl3
liquid film
4880 A,200 M,liquid
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