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MS-NW-7460 p-decylaniline C16H27N (Mass of molecular ion: 233)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 1.1 28.0 1.1 29.0 2.0 39.0 1.0 41.0 2.5 43.0 1.8 55.0 1.0 77.0 2.2 78.0 1.1 79.0 1.3 93.0 1.0 106.0 100.0 107.0 8.7 119.0 1.6 120.0 1.1 233.0 13.8 234.0 2.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C16 H27 N 0.036 g : 0.5 ml CDCl3 p-decylaniline Assign. Shift(ppm)
A 6.97 B 6.62 C 3.5 D 2.48 E 1.57 F 1.34 to 1.15 G 0.88
Hz ppm Int.
628.25 7.015 94 626.13 6.992 48 624.63 6.975 43 619.88 6.922 146 617.31 6.893 37 596.38 6.660 138 594.25 6.636 55 589.75 6.585 51 588.00 6.566 81 230.13 2.570 40 228.38 2.551 33 227.94 2.546 33 223.25 2.493 79 215.63 2.408 66 145.94 1.630 34 142.63 1.593 41 142.38 1.590 41 140.31 1.567 49 139.63 1.560 49 137.25 1.533 51 136.69 1.527 50 135.13 1.509 46 134.00 1.497 46 133.31 1.489 46 131.13 1.465 51 130.06 1.453 53 129.75 1.449 53 125.81 1.405 71 112.44 1.256 1000 93.56 1.045 33 92.44 1.033 33 90.44 1.010 31 83.44 0.932 92 82.31 0.920 83 80.94 0.904 88 78.56 0.878 186 75.75 0.846 69 72.81 0.813 61
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