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MassMS-NW-7300 2,4-difluorophenol C6H4F2O (Mass of molecular ion: 130)
Source Temperature: 200 °C Sample Temperature: 190 °C Reservoir, 75 eV
31.0 4.7 37.0 1.2 38.0 1.2 41.0 1.3 50.0 3.2 51.0 5.5 52.0 1.3 53.0 2.1 55.0 2.7 56.0 3.8 57.0 5.5 61.0 2.4 62.0 2.3 63.0 10.2 65.0 4.4 68.0 1.3 74.0 1.4 75.0 6.0 76.0 1.6 80.0 1.4 81.0 13.6 82.0 73.5 83.0 6.1 99.0 2.1 100.0 1.2 101.0 17.2 102.0 2.9 110.0 7.0 129.0 2.6 130.0 100.0 131.0 7.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H4 F2 O 0.05 ml : 0.5 ml CDCl3 2,4-difluorophenol 
Assign. Shift(ppm)
A 6.937 B 6.826 C 6.743 D 5.80
Hz ppm Int.2789.79 6.981 31 2784.91 6.969 604 2779.54 6.955 640 2775.63 6.946 832 2775.27 6.945 781 2772.34 6.937 107 2770.26 6.932 831 2769.78 6.931 785 2765.99 6.922 735 2760.50 6.908 716 2746.83 6.874 30 2739.26 6.855 646 2736.33 6.847 736 2733.52 6.840 90 2730.96 6.834 676 2728.15 6.827 1000 2725.59 6.820 763 2722.90 6.814 79 2722.17 6.812 79 2719.97 6.806 620 2717.29 6.800 737 2713.99 6.791 46 2711.67 6.786 37 2710.94 6.784 34 2709.72 6.781 41 2709.11 6.779 42 2704.71 6.768 597 2703.00 6.764 596 2701.78 6.761 531 2700.07 6.757 522 2698.24 6.752 122 2696.66 6.748 653 2695.80 6.746 603 2694.95 6.744 700 2693.97 6.741 773 2692.87 6.739 536 2692.02 6.736 603 2691.04 6.734 499 2687.74 6.726 476 2686.04 6.721 480 2684.69 6.718 418 2682.98 6.714 409 2320.19 5.806 155
in CDCl3
liquid film
4880 A,200 M,liquid
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