3-Chloro-4-fluoroaniline

Mass

MS-IW-9157          
3-chloro-4-fluoroaniline
C6H5ClFN            (Mass of molecular ion:    145)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.0
      28.0       3.9
      31.0       3.1
      36.0       1.3
      37.0       1.8
      38.0       2.1
      39.0       2.4
      41.0       2.0
      44.5       1.7
      50.0       1.8
      51.0       1.5
      52.0       3.1
      54.5       5.0
      55.0       1.5
      56.0       2.6
      57.0       7.6
      61.0       2.3
      62.0       3.4
      63.0       6.0
      64.0       1.5
      65.0       1.4
      67.0       1.7
      69.0       1.2
      72.5       6.5
      73.0       1.7
      73.5       2.5
      74.0       1.3
      80.0       1.0
      81.0       4.7
      82.0       6.5
      83.0      34.8
      84.0       3.4
      89.0       2.7
      90.0       6.5
      91.0       2.3
      93.0       1.8
      98.0       1.2
     108.0       2.6
     109.0       7.6
     110.0      13.2
     111.0       1.1
     117.0       6.7
     118.0       9.6
     119.0       2.9
     120.0       3.4
     125.0       1.6
     144.0       2.4
     145.0     100.0
     146.0       7.8
     147.0      31.9
     148.0       2.3

Assign. Shift(ppm) A 6.907 B 6.676 C 6.488 D 3.59

     Hz     ppm     Int.

   2769.41   6.930    514
   2760.62   6.908   1000
   2751.71   6.886    554
   2672.73   6.688    517
   2669.92   6.681    564
   2666.63   6.673    521
   2663.82   6.666    548
   2600.46   6.507    325
   2597.66   6.500    339
   2596.68   6.498    360
   2593.87   6.491    313
   2591.67   6.485    302
   2588.87   6.478    308
   2588.01   6.476    326
   2585.08   6.469    268
   1435.79   3.593    218