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MS-NW-9704 2,5-dibromoaniline C6H5Br2N (Mass of molecular ion: 249)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
37.0 1.7 38.0 2.8 39.0 1.9 41.0 2.1 44.5 3.3 45.0 1.4 45.5 6.5 52.0 6.5 61.0 3.0 62.0 5.4 63.0 12.6 64.0 5.9 65.0 2.9 74.0 1.6 84.5 3.3 85.0 2.0 85.5 3.2 86.0 2.1 89.0 1.3 90.0 32.1 91.0 17.9 92.0 1.8 117.0 1.1 119.0 1.1 124.5 2.5 125.5 4.9 126.5 2.3 143.0 5.7 145.0 5.3 169.0 2.0 170.0 19.4 171.0 4.3 172.0 18.7 173.0 2.2 249.0 51.3 250.0 3.9 251.0 100.0 252.0 7.1 253.0 48.4 254.0 3.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H5 Br2 N 0.038 g : 0.5 ml CDCl3 2,5-dibromoaniline Assign. Shift(ppm)
A 7.235 B 6.889 C 6.723 D 4.13
Hz ppm Int.
2896.00 7.247 882 2894.04 7.242 39 2892.33 7.238 24 2891.36 7.235 29 2887.57 7.226 967 2758.42 6.903 27 2754.39 6.893 919 2751.95 6.886 1000 2747.92 6.876 21 2691.89 6.736 728 2689.70 6.731 694 2686.77 6.723 32 2683.47 6.715 723 2681.27 6.710 570 2678.34 6.702 22 2677.98 6.701 23 1651.25 4.132 151
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