azidopyrene

Mass

MS2004-02557WA      
1-pyrenyl azide
C16H9N3             (Mass of molecular ion:    243)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 70 eV

      28.0      11.2
      62.0       1.3
      63.0       2.4
      68.0       1.2
      72.0       1.5
      74.0       2.0
      75.0       1.2
      80.0       1.2
      80.5       1.9
      81.0       3.9
      81.5       2.1
      86.0       2.0
      87.0       3.2
      88.0       1.0
      93.0       7.5
      93.5      37.6
      94.0      30.3
      94.5       8.0
      95.0       1.3
      98.0       1.5
      99.0       1.7
     100.0       3.3
     100.5       1.1
     106.5       2.5
     107.0       5.5
     107.5      34.0
     108.0       6.1
     108.5       3.5
     110.0       1.1
     111.0       1.4
     161.0       1.9
     162.0       1.7
     163.0       3.3
     164.0       1.7
     185.0       1.4
     186.0       3.0
     187.0      12.9
     188.0      11.1
     189.0      10.7
     190.0       2.0
     200.0       1.4
     201.0       1.0
     212.0       6.5
     213.0       5.9
     214.0      82.0
     215.0     100.0
     216.0      19.3
     217.0      17.3
     218.0       2.9
     243.0      22.8
     244.0       4.2

Assign. Shift(ppm) A 8.193 B *1 8.113 C *1 8.106 D 8.052 E 7.99 F 7.962 G *2 7.94 J *2 7.92 K 7.698

     Hz     ppm     Int.

   3280.16   8.205    516
   3271.00   8.182    646
   3247.44   8.124    356
   3245.12   8.118    332
   3237.43   8.098    470
   3223.27   8.063    516
   3215.09   8.043    571
   3200.57   8.006    595
   3191.17   7.983    857
   3183.35   7.963    659
   3175.79   7.944    355
   3170.42   7.931   1000
   3161.50   7.909    170
   3081.18   7.708    731
   3073.00   7.687    648