400 MHz in D2O
-
1H NMR 399.65 MHz C6 H12 O5 0.038 g : 0.5 ml D2O 6-deoxy-D-galactose Assign. Shift(ppm)
A 5.204 B 4.556 C 4.202 D 3.86 to 3.75 E 3.638 F 3.450 G 1.249 J 1.209 MIXTURE OF ANOMERS THE SOLVENT SIGNAL SUPPRESSED ASSIGNED BY H-H COSY
Hz ppm Int.
2081.79 5.210 313 2077.88 5.200 319 1824.83 4.567 187 1816.89 4.547 193 1689.45 4.228 60 1689.09 4.227 61 1686.65 4.221 33 1682.74 4.211 178 1679.32 4.202 46 1676.03 4.194 178 1669.56 4.178 62 1549.56 3.878 153 1546.26 3.870 192 1542.11 3.859 50 1539.18 3.852 237 1535.89 3.844 351 1527.47 3.823 123 1524.90 3.816 373 1524.05 3.814 394 1521.48 3.808 269 1521.12 3.807 269 1520.63 3.805 274 1511.96 3.784 318 1508.06 3.774 281 1504.15 3.764 51 1501.59 3.758 198 1497.80 3.748 245 1495.61 3.743 254 1490.23 3.729 64 1488.28 3.724 69 1461.18 3.657 97 1457.76 3.648 81 1451.29 3.632 122 1447.75 3.623 105 1387.08 3.471 108 1379.15 3.451 107 1377.20 3.447 99 1369.26 3.427 77 502.69 1.258 504 496.09 1.242 511 490.60 1.228 118 486.57 1.218 1000 479.98 1.202 972
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