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MS-IW-8221 1,2-dibromo-1-fluoroethane C2H3Br2F (Mass of molecular ion: 204)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 3.7 27.0 2.3 31.0 1.1 44.0 3.3 45.0 21.5 46.0 9.3 79.0 2.0 81.0 2.1 93.0 2.0 95.0 1.5 105.0 21.4 106.0 1.6 107.0 20.8 111.0 2.4 113.0 2.4 124.0 1.7 125.0 100.0 126.0 3.7 127.0 98.3 128.0 2.3 186.0 1.4 204.0 1.6 206.0 3.3 208.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C2 H3 Br2 F 0.05 ml : 0.5 ml CDCl3 1,2-dibromo-1-fluoroethane Assign. Shift(ppm)
A 6.517 B *1 3.938 C *1 3.840
Hz ppm Int.
2635.25 6.594 632 2632.57 6.588 692 2626.71 6.573 640 2624.02 6.566 677 2584.72 6.468 669 2582.15 6.462 700 2576.05 6.446 664 2573.49 6.440 667 1592.16 3.984 442 1583.74 3.963 418 1580.44 3.955 1000 1574.95 3.941 40 1574.58 3.940 40 1571.90 3.934 919 1568.48 3.925 779 1559.94 3.904 787 1554.93 3.891 843 1552.37 3.885 849 1543.21 3.862 459 1540.65 3.855 439 1526.49 3.820 809 1523.93 3.814 821 1514.77 3.791 563 1512.21 3.784 538
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