3-Pyridinecarboxylic acid N-hydroxymethylamide
Product Name 3-Pyridinecarboxylic acid N-hydroxymethylamide
CAS3569-99-1
MFC7H8N2O2
MW152.15
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MassMS-NW-9975 N-(hydroxymethyl)nicotinamide C7H8N2O2 (Mass of molecular ion: 152)
Source Temperature: 160 °C Sample Temperature: 100 °C Direct, 75 eV
17.0 1.3 18.0 6.7 26.0 2.1 27.0 2.1 28.0 9.4 29.0 25.0 30.0 24.5 31.0 1.3 37.0 1.0 38.0 1.9 39.0 3.4 44.0 8.7 46.0 1.3 49.0 1.9 50.0 12.7 51.0 35.0 52.0 13.4 53.0 3.1 75.0 1.5 76.0 2.7 77.0 7.1 78.0 76.8 79.0 15.7 80.0 1.0 94.0 4.9 104.0 2.6 105.0 7.2 106.0 70.9 107.0 8.3 122.0 100.0 123.0 11.9 152.0 1.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H8 N2 O2 0.040 g : 0.5 ml DMSO-d6 N-(hydroxymethyl)nicotinamide 
Assign. Shift(ppm)
A 9.38 B 9.064 C 8.739 D 8.241 E 7.537 F 5.84 G 4.767
Hz ppm Int.3752.90 9.391 106 3747.10 9.376 184 3741.15 9.362 107 3623.81 9.068 519 3623.05 9.066 560 3621.52 9.062 557 3620.76 9.060 516 3496.09 8.748 445 3494.42 8.744 472 3491.36 8.737 471 3489.69 8.732 463 3299.87 8.257 269 3298.03 8.253 343 3295.90 8.247 266 3291.93 8.238 291 3290.10 8.233 355 3289.64 8.232 351 3287.96 8.228 272 3018.95 7.554 313 3018.19 7.553 311 3014.22 7.543 307 3013.31 7.540 311 3011.02 7.535 307 3010.25 7.533 300 3006.13 7.522 284 3005.37 7.521 286 2338.71 5.852 367 2332.00 5.836 878 2328.03 5.826 34 2325.13 5.818 399 1911.77 4.784 632 1905.21 4.768 1000 1898.65 4.751 626
in DMSO-d6
in D2O
KBr disc
nujol mull
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