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MassMS-IW-4771 allyl methyl carbonate C5H8O3 (Mass of molecular ion: 116)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 30.8 18.0 1.0 26.0 4.5 27.0 17.0 28.0 8.7 29.0 32.4 30.0 5.2 31.0 8.9 32.0 1.7 33.0 5.5 37.0 2.9 38.0 6.2 39.0 52.8 40.0 14.8 41.0 100.0 42.0 33.8 43.0 5.7 44.0 24.5 45.0 17.8 55.0 3.9 56.0 2.8 57.0 78.2 58.0 2.8 59.0 62.7 60.0 2.7 71.0 54.0 72.0 33.0 73.0 1.6 77.0 13.5 84.0 7.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H8 O3 0.05 ml : 0.5 ml CDCl3 allyl methyl carbonate 
Assign. Shift(ppm)
A 5.936 B 5.359 C 5.263 D 4.628 E 3.786
Hz ppm Int.2392.58 5.987 56 2386.84 5.973 112 2382.08 5.961 60 2381.10 5.958 64 2376.34 5.947 115 2375.37 5.944 76 2370.73 5.933 68 2369.63 5.930 133 2364.99 5.918 68 2363.89 5.915 74 2359.13 5.903 123 2353.52 5.889 68 2152.34 5.386 78 2150.76 5.382 176 2149.29 5.378 179 2147.83 5.375 79 2135.13 5.343 68 2133.54 5.339 155 2132.08 5.335 156 2130.62 5.332 69 2110.47 5.281 82 2109.25 5.278 179 2107.91 5.275 171 2106.69 5.272 78 2100.10 5.255 72 2098.75 5.252 157 2097.41 5.249 161 2096.19 5.246 77 1853.88 4.639 261 1852.66 4.636 310 1852.29 4.635 302 1851.07 4.632 249 1848.14 4.625 243 1846.92 4.622 293 1846.56 4.621 296 1845.34 4.618 246 1519.17 3.802 32 1513.18 3.787 1000 1510.01 3.779 96
in CDCl3
liquid film
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