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1,1'-Thiobisethane

Product Name 1,1'-Thiobisethane

CAS352-93-2

MFC4H10S

MW90.19

¹³CNMR

Mass

MS-NW-2557          
diethyl sulfide
C4H10S              (Mass of molecular ion:     90)

   Source Temperature: 290 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      26.0       4.2
      27.0      30.8
      28.0       8.2
      29.0      35.9
      34.0       3.8
      35.0      11.4
      41.0       8.2
      44.0       1.2
      45.0      11.9
      46.0      12.3
      47.0      69.7
      48.0       1.9
      49.0       3.0
      57.0       1.7
      58.0       5.0
      59.0       8.3
      60.0      10.4
      61.0      51.1
      62.0      46.8
      63.0       3.5
      64.0       2.0
      75.0     100.0
      76.0       4.0
      77.0       4.5
      89.0       3.3
      90.0      75.3
      91.0       4.2
      92.0       3.5

parameter in CDCl3

¹H NMR	300 MHz
C₄ H₁₀ S	11.0 mol% in CDCl₃
diethyl sulfide

    Parameter     ppm  Hz

      D(A)         1.256
      D(B)         2.547
       J(A,B)          7.40

     Hz     ppm     Int.

    775.30   2.584    153
    767.90   2.560    474
    760.50   2.535    492
    753.12   2.510    171
    384.13   1.280    508
    376.74   1.256   1000
    369.34   1.231    469

in CDCl3

liquid film

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