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S-(p-Methoxybenzoyl)thiohydroxylamine

Product Name S-(p-Methoxybenzoyl)thiohydroxylamine

CAS35124-66-4

MFC8H9NO2S

MW183.23

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  • Mass 

    MS-NW-7309          
S-(p-methoxybenzoyl)thiohydroxylamine
C8H9NO2S            (Mass of molecular ion:    183)


       Source Temperature: 210 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          38.0       1.9
      48.0       1.5
      50.0       3.0
      51.0       1.6
      62.0       1.3
      63.0       5.4
      64.0       7.1
      74.0       1.3
      75.0       1.0
      76.0       2.3
      77.0      20.9
      78.0       1.7
      79.0       1.1
      92.0      13.7
      93.0       1.2
     107.0       9.8
     108.0       1.0
     135.0     100.0
     136.0       9.1
     139.0       1.8

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 N O2 S 0.024 g : 0.5 ml CDCl3
    S-(p-methoxybenzoyl)thiohydroxylamine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.850
      B             6.943
      C             3.867
      D             2.75
  

         Hz     ppm     Int.


       3144.53   7.869     31
   3141.72   7.862    265
   3139.65   7.857     82
   3134.89   7.845     84
   3132.69   7.839    278
   3129.88   7.832     35
   2781.98   6.962     30
   2779.17   6.955    238
   2776.98   6.949     74
   2772.22   6.937     70
   2770.14   6.932    226
   2767.33   6.925     29
   1549.93   3.879     21
   1545.53   3.868   1000
   1097.78   2.747     73

in CDCl3



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