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MassMS-NW-5735 di-tert-pentyl disulfide C10H22S2 (Mass of molecular ion: 206)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 5.2 29.0 9.8 39.0 4.8 41.0 13.0 42.0 2.9 43.0 64.2 44.0 2.2 45.0 1.1 53.0 1.5 55.0 11.4 56.0 1.1 57.0 5.7 59.0 2.3 61.0 1.1 69.0 2.6 70.0 3.6 71.0 100.0 72.0 5.6 73.0 1.0 85.0 3.6 103.0 2.1 107.0 1.2 122.0 1.2 136.0 8.8 168.0 2.4 206.0 6.0
parameter in CDCl3
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1H NMR 300 MHz C10 H22 S2 0.05 ml : 0.5 ml CDCl3 di-tert-pentyl disulfide 
Parameter ppm Hz
D(A) 1.573 D(C) 0.935 J(A,C) 7.45 D(B) 1.242
Hz ppm Int.483.23 1.611 28 475.76 1.586 97 468.31 1.561 104 460.95 1.536 36 372.60 1.242 1000 287.79 0.959 112 280.37 0.935 217 272.93 0.910 94
in CDCl3
liquid film
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